Rhenium oxide nanoparticles have been prepared using ultrasonication at 20 kHz. Samples characterization was committed via SEM-EDX, TEM, XRD, and Raman spectroscopy. Various experimental parameters were examined, including precursor/substrate amounts, ultrasonication intensity, and type of solvent used. Insights to the agglomeration of the prepared nanoparticles depending on the preparation parameters

Scaling is a major problem in the thermal desalination operation which is mainly attributed to the deposition of salts on the tube, thereby increasing the resistance to heat transfer. To reduce or prevent the formation of scale on heat transfer surfaces, treating desalination concentrates and precipitating sparingly soluble salts can be a promising method. In the present work, the effect of ultrasound

The potential of ultrasound as a process intensification technique in the extraction of lead from a landfilled metallurgical residues is explored. The silent or non-sonicated process makes use of acidic sodium chloride as the leachate with lead leaching in the range of 45% if a three-stage process is followed. The mixture was sonicated in a batch setup manufactured in-house. The yield obtained in silent

When an aqueous Au(III) solution containing 1-butanol was sonicated under Ar, Au(III) was reduced to Au(0) to form Au particles. This is because various reducing species are formed during sonication, but the reactivity of these species has not yet been evaluated in detail. Therefore, in this study, we analyzed the effects of Au(III) on the rates of the formation of gaseous and water-soluble compounds

In green approaches for electrocatalyst synthesis, sonochemical methods play a powerful role in delivering the abundant surface areas and nano-crystalline properties that are advantageous to electrocatalytic detection. In this article, we proposed the sphere-like and perovskite type of bimetal oxides which are synthesized through an uncomplicated sonochemical procedure. As a yield, the novel calcium

In the present work, the accelerated ageing process of sherry vinegar has been studied at pilot scale by means of the joint application of ultrasound, micro-oxygenation and wood chips (American oak, French oak and Spanish oak). The CIELab parameters have been studied as well as the polyphenolic and volatile content of the aged vinegar samples. Vinegars aged with American oak presented different chromatic

We investigated the effect of ultrasound-assisted pH shift treatment on the micro-particle, molecular, and spatial structure of rapeseed protein isolates (RPI). Various ultrasonic frequency modes (fixed, and sweep) was used. Protein characterization by the indexes: particle size, zeta potential, sodium dodecyl sulfate polyacrylamide gel electrophoresis (SDS-PAGE), scanning electron microscopy (SEM)

The sonochemical formation of Au seeds and their autocatalytic growth to Au nanorods were investigated in a one-pot as a function of concentration of HAuCl4, AgNO3, and ascorbic acid (AA). The effects of ultrasonic power and irradiation time were also investigated. In addition, the formation rate of Au nanorods was analyzed by monitoring the extinction at 400 nm by UV–Vis spectroscopy and compared

The influence of the sample morphology and experimental conditions towards the sonochemical dissolution of nanoscale ThO2 samples in sulfuric acid media is described. Significant sonochemical dissolution rates and yields are observed at 20 kHz under Ar/O2 atmosphere in dilute 0.5 M H2SO4 at room temperature, contrasting with the generally-reported high refractory behavior for ThO2. The dissolution

When liquids flow in the pipelines, the onset of cavitation can be characterized by a variant of the Euler number known as the cavitation number (CN), which is based on the velocity and denoted by C in this paper. Conventionally, cavitation is considered to be induced when C ~ 1. However, experimental observations and several pipe bursts indicate that the CN may incorrectly predict the onset of cavitation

The present study investigates the wastewater treatment performance of an acoustic cavitation assisted plasma (ACAP) process in a circulating reactor using Rhodamine B (RhB) as a model water pollution. The concept of this process was proposed by the authors recently for a batch type rector. The measurements revealed that combining the ultrasound irradiation with pulsed discharge plasma allows the RhB

The influence of ultrasonic frequency (20 kHz) and glucose pretreatments either alone or in combination on the drying of sweet potato slices (3 mm) using a hot-air dryer at 60 °C was tested to study the kinetics modeling, phytochemicals, antioxidant activities, and functional and textural changes of the final dried product. The results indicated that total phenolic content and total flavonoid content

Sonolysis has been proposed as a promising treatment technology to remove per- and polyfluoroalkyl substances (PFASs) from contaminated water. The mechanism of degradation is generally accepted to be high temperature pyrolysis at the bubble surface with dependency upon surface reaction site availability. However, the parametric effects of the ultrasonic system on PFAS degradation are poorly understood

Nowadays celiac disease is becoming more common. It is the autonomic genetic disease that is accompanied by damage to the intestines due to a reaction to eating some proteins. People who are suffering from celiac disease cannot eat food containing gluten, including dough made from gluten-containing seeds. But the gluten-free dough has commonly bad rheological properties and cannot be used for automatic

Oryza sativa L. ‘Violet Nori’ is an Italian cultivar of spontaneous growing aromatic purple rice which is particularly rich in polyphenolic compounds, especially anthocyanins, conferring it an excellent antioxidant capacity. The present study aimed at increasing the extraction yields of its antioxidant compounds with green strategies and it is divided into two steps. The first step concerned a solubility

The near-solid wall multi-bubble cavitation is an extremely complex phenomenon, and cavitation has strong erosiveness. The melting point (about 3410 °C) of tungsten is highest among all pure metals, and its hardness is also very high (its yield strength is greater than 1 GPa). What would happen to pure tungsten wire under extreme conditions caused by collapsing cavitation bubbles at high hydrostatic

This work investigates the effect of sonication on brown and milled rice grains of both waxy and non-waxy varieties. We report herein the microstructural analysis of uncooked rice kernels under sonication and its effect on the textural properties. X-ray computed tomography results showed the formation of microporous surfaces and the creation of cracks and fissures. Sonication increased the % porosity

The effect of ultrasound on the conformational and physicochemical properties of soy protein isolate hydrolysates (SPHs) was investigated. SPHs were prepared at hydrolysis times of 20 min, 60 min, and 180 min, then treated with ultrasound for 10 min, 20 min, and 30 min at a frequency of 20 kHz and output powers of 150 W and 450 W. The structural properties and antioxidant capacities of the aqueous

Ultrasound is an emerging and promising method for demulsification, which is highly affected by acoustic parameters and emulsion properties. Herein, a series of microscopic and dehydration experiments are carried out to investigate the parameter optimization of ultrasonic separation. The results show that the optimal acoustic parameters highly depend on the emulsion properties. For low frequency ultrasonic

In this study, ultrasound-assisted vacuum drying (UAVD) was employed as a new approach to improve the efficiency and produce dried hawthorn fruit juice powders with acceptable quality. To achieve these goals, the effects of ultrasound intensity (at four levels of 15.29, 20.38, 22.93 and 24.46 kW/m2) were evaluated. The results showed that UAVD significantly shortened the drying time (P < 0.05), and

Bubble behaviors near a boundary in an ultrasonic field are the fundamental forms of acoustic cavitation and of substantial importance in various applications, such as industry cleaning, chemical engineering and food processing. The effects of two important factors that strongly affect the dynamics of a single acoustic cavitation bubble, namely, the initial bubble radius and the standoff distance,

Graphitic carbon nitride (g-C3N4) is an analog of graphite due to its unique electronic structure. g-C3N4 based materials have been used in photocatalytic applications. However, pure g-C3N4 suffers from major shortcomings which include poor disparity, low surface area and a high recombination rate of photo generated electron-hole pairs that significantly reduce its photocatalytic activity. In this

An amphiphilic metallo-supramolecular poly(propylene glycol)-block-poly(ethylene glycol) block copolymer containing a bis(2,2′:6′,2″-terpyridine) ruthenium (II) complex as a supramolecular connection between the two constituting blocks was used to prepare stable aqueous micelles which displayed a high intensity focused ultrasound (HIFU) triggered release behavior. By adjusting the HIFU time and intensity

Freezing is one of the most efficient preservation approaches applied to food products and thawing is the reverse process of freezing. However, traditional freezing / thawing methods have low process efficiency. The application of ultrasound is a potential supplementary technique to improve the performance of both freezing and thawing processes of foods. Application of power ultrasound is able to better

In this paper, the crystallization of L-glutamic acid with application of ultrasound was explored in detail, including the process of nucleation, polymorphic control and polymorphic transformation. The induction time and metastable zone widths (MSZWs) were measured with and without ultrasound during the nucleation process. The induction time and MSZWs were decreased by ultrasound and the induction

The initial motivation for the study was to gain deeper understanding into the background of emulsion preparation by ultrasound (cavitation). In our previous work (Perdih et al., 2019) we observed rich phenomena occurring near the liquid-liquid interface which was exposed to ultrasonic cavitation. Although numerous studies of bubble dynamics in different environments (presence of free surface, solid

A highly viscous nature of heavy oil poses challenges to transportation leading to costly operation and difficult processing. Traditional methods of upgrading unconventional hydrocarbon sources involve catalytic and thermal upgrading and these methods require high temperature and pressure. In the present study, partial upgrading of heavy hydrocarbon is studied by using cavitation and the stimulator

Ultrasonic-assisted ultrafiltration (UAU) removing bacterial endotoxin from diammonium glycyrrhizinate, was firstly applied to surfactant separation. Separation efficiency was related with four variables, including ultrafiltration molecular weight cut off (MWCO), ultrasonic power, concentration and pH. The SCQ-9200E ultrasonic system was provided for the study with adjustable ultrasonic power 80 W

Although the factors that influence ultrasonic cavitation erosion in solid particle suspensions have been extensively studied, the role that solid particles play in the cavitation process remains poorly understood. The ultrasonic cavitation erosion of AISI 1045 carbon steel was studied in the presence of monodisperse silica particles (10–100 μm, 0.5–20 vol%) suspended in transformer oil. Based on our

In the present study, Proteus vulgaris lipase (PVL) was engineered using directed evolution to increase methanol tolerance so that it would be more tolerant and efficient for harsh conditions employed in biodiesel synthesis, which is limiting their industrial use. The influence of ultrasound under different experimental conditions on the biodiesel conversion yield using methanolysis of non-edible neem

The effect of particle size on sonochemical desorption, degradation and change in bioaccessibility of polycyclic aromatic hydrocarbons (PAHs) on contaminated sediments was investigated. Batch experiments were performed with the whole sediment (WS < 850 μm), a large size range fraction (150 μm < LSR < 850 μm), and a small size range fraction (SSR < 150 μm) of the whole sediment. PAH degradation followed

Hybrid nanoparticles (HNPs) with zinc oxide and polymethyl metha acrylate (inorganic/ polymer) were synthesized through the exploitation of ultrasound approach. The synthesized HNPs were further characterized employing transmission electron microscopy and x-ray diffraction. ZnO-PMMA based HNPs exhibit excellent protection properties to mild steel from corrosion when gets exposed to acidic condition

Lotus seed starch nanoparticles were prepared by ultrasonic (ultrasonic power: 200 W, 600 W, 1000 W; time: 5 min, 15 min, 25 min; liquid ratio (starch: buffer solution): 1%, 3%, 5%) assisted enzymatic hydrolysis (LS-SNPs represent lotus seed starch nanoparticles prepared by enzymatic hydrolysis and U-LS-SNPs represent lotus seed starch nanoparticles prepared by high pressure homogenization-assisted

Protein is one of the most abundant natural polymeric materials, but only a few studies on nanoproteins have been conducted. In this paper, a novel approach based on ultrasound-assisted enzymatic hydrolysis was employed for the preparation of microkeratin and nanokeratin from wool. The hydrolysis system included a solution containing enzyme (esperase) and reductant (L-cysteine) and treated ultrasonically

Ozonation (OZ) is an important advanced oxidation process to purify water and wastewater. Because of the lower solubility and instability of ozone (O3), selective oxidation and dependence on pH value, the industrial applications of OZ have been hindered by the following disadvantages: incomplete removal of pollutants, lower mineralization efficiency and the formation of toxic by-products. Meanwhile

The waste sludge from shipping docks contains important elements that can be used as a catalyst after proper processing. The purpose of this study was to remove of amoxicillin (AMX) from the aquatic environment using waste sludge from shipping docks as catalyst in the presence of hydrogen peroxide/ultrasound waves. The catalyst was produced by treating waste sludge at 400 °C for 2 h. N2 adsorption

The aim of this study was to develop an effective method for extracting anthocyanins from blueberry Vaccinium spp. (ABVS) using freeze-ultrasonic thawing technology (FUTE). Various parameters including freezing time, ultrasonic time, ultrasonic temperature and liquid–solid ratio were optimized by a single-factor design and multiple response surface methodology. The amounts of extracted anthocyanin

To meet the objectives of the Intergovernmental Panel on Climate Change nations are adopting policies to encourage consumers to purchase electric vehicles. Electrification of the automobile industry reduces greenhouse gases but active metals for the cathode—LiCoO2 and LiNiO2—are toxic and represent an environmental challenge at the end of their lifetime. LiFePO4 (LFP) is an attractive alternative that

Acoustic noise spectra were studied for the first time in overheated water using sonohydrothermal reactor operating at 20 kHz ultrasound in the temperature range from 25 to 200°C at the autogenic pressure of 1-14 bar. The obtained results highlighted a dominating role of stable cavitation during ultrasonic treatment of hot water. Heating of sonicated water results in the formation of large number of

Most scientists consider that sonochemistry became recognised as a discrete subject in the 1980’s – some 40 years ago which coincidentally is when my own interests in the subject began. This review briefly outlines how I first became involved in sonochemistry and then in its development. However its main theme is the way in which my links with China through sonochemistry have developed from their beginnings

Stent placement is an effective treatment for atherosclerosis, but is suffered from in-stent restenosis (ISR) caused by stent mechanical damage. Conventional ISR treatment such as drug-eluting stents (DES) is challenged by the low therapeutic efficacy and severe complications, unchangeable drug dosage for individuals, and limited drug penetration in the vascular tissue. We hypothesize that magnetic

In this paper, the cavitation performance and corresponding pressure pulsation, noise and vibration induced by the choked cavitating flow in a Venturi reactor are investigated experimentally under different cavitation conditions by using high-speed camera and high frequency sensors. Based on the instantaneous continuous cavitation images, the Proper Orthogonal Decomposition (POD), a tool to analyze