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Recent Advances in Iodine‐Mediated Radical Reactions Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-02-12 Wen Yang, Jian Guo, Samual Hee, Yu Chen
Over the past two decades, iodine‐mediated free radical reactions have been extensively explored and employed in chemical transformations that complement traditional ionic reactions. In this review, we have updated the progress of the iodine‐mediated radical reactions in organic synthesis reported between 2015 and mid‐2024, and organized the reactions according to their mechanistic pathways. In general
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Cobalt/Salox‐catalyzed Stereoselective C‐H Functionalization: Enantioselective Construction of Axially Chiral Cyclic Phosphinamides with P‐Stereogenic Center Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-02-12 Bo Jiang, Hui Wang, Xiaobin Sun, Yiyang Qiao, Xiufang Xu, Zhiwei Miao
We describe a novel cobalt/salicyloxazoline (Salox) catalytic system for enantioselective C‐H functionalization, enabling the synthesis of P‐stereogenic and axially chiral cyclic phosphinic amides. Chiral Salox ligands, conveniently prepared in a single step from salicylonitriles and chiral amino alcohols, facilitated this transformation with excellent enantioselectivities (92‐99% ee) and moderate
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Recent advancements in the synthesis of sulfonyl fluorides with heterocyclic skeletons Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-02-11 Yi-Chen Dong, Li-Jing Wang
Sulfonyl fluoride compounds, particularly those with heterocyclic skeletons, have gained increasing attention due to their widespread applications in organic synthesis, drug discovery, and the life sciences. Consequently, the exploration of efficient and diverse approaches for synthesizing sulfonyl fluorides with heterocyclic skeletons has garnered significant interest from organic chemists. In recent
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Aldehyde Dehydrogenase from Klebsiella pneumoniae: A Robust Biocatalyst for Preparing Heteroatom‐Containing Carboxylic Acids Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-02-11 Yuchen Han, Nan Geng, Jiangtao Sha, Huanhuan Li, Chun You, Weidong Liu, Jie Zhang, Jianjun Shi, Xin Wu, Wuyuan Zhang
Heterocyclic scaffolds have broad applications in organic synthesis, resulting in the production of essential compounds utilized in pharmaceuticals, agrochemicals, and dietary products. In this study, we present the characterization of a discovered succinic semialdehyde dehydrogenase from Klebsiella pneumoniae (KpSSADH) and elucidate its crystallographic structure. Further investigation into the catalytic
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Effective and Practical Stereoselective Synthesis of Nutlins Precursors by Immobilization of Privileged Chiral Mono‐Amidine Catalyst Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-02-11 Sofia Toldo, Lorenzo Poletti, Graziano Di Carmine, Olga Bortolini, Carmela De Risi, Simona Felletti, Greta Compagnin, Alessandro Massi, Daniele Ragno
A strategy for the immobilization of Johnston’s Mono(AMidine) catalyst (MAM) onto polystyrene, silica and hybrid silica‐polystyrene nanoparticles is presented. The catalyst activity was evaluated in the stereoselective aza‐Henry reaction leading to the pivotal β‐amino nitroalkane precursors of the anti‐cancer agents Nutlins (with Nutlin‐3a as the most active drug). The effect of the support and the
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Unveiling the Potential of a Cobalt‐Based Metal‐Organic Framework in Carbodiimide Synthesis Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-02-06 Daniël S. Verdoorn, Alessio Zuliani, Prabhat Ranjan, Juan P. Holgado, Noureddine Khiar, Jordy Saya, Carolina Carrillo-Carrión, Bert Maes, Romano Orru
The synthesis of carbodiimides via nitrene transfer to isocyanides has garnered significant attention in recent years. However, this reaction predominantly relies on homogeneous catalytic systems with high catalyst loadings. In this study, we employed ZIF‐67 MOF as a heterogeneous catalyst for carbodiimide synthesis and conducted an in‐depth analysis of its stability. Our findings reveal the non‐innocent
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Rh(III)‐Catalyzed C(sp2)–H and C(sp2)–C(sp2) Bond Activation of Aryl Oximes with CF3‐Imidoyl Sulfoxonium Ylides: Access to N‐(2‐Cyanoaryl)‐3‐(Trifluoromethyl)isoquinolin‐1(2H)‐Imines Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-02-05 pinyi li, Jian Chen, Zuguang Yang, Zhengkai Chen
A rhodium(III)‐catalyzed redox‐neutral C‐H and C‐C bond activation reaction of aryl oximes and CF3‐substituted imidoyl sulfoxonium ylides (TFISYs) has been described, producing a wide variety of N‐(2‐cyanoaryl)‐3‐(trifluoromethyl)isoquinolin‐1(2H)‐imines in moderate to excellent yields. The transformation might involve a consecutive C(sp2)–H bond activation, intramolecular spiro‐cyclization, C‐C bond
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Second‐Generation One‐pot Enantioselective Heck‐Matsuda Arylations of Unactivated Olefins Directly from Anilines and Nitroarenes Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-02-05 Carlos Roque Correia, Luiz Leão, Valdeir Oliveira, Tomaz Henrique Duarte Chorro, Sergei Gorbatov
A highly improved second generation of the one‐pot enantioselective Heck‐Matsuda reaction directly from anilines and nitroarenes is reported. This practical arylation method, featuring 56 examples, relies on the in situ diazotization of anilines and 3‐aminothiophenes, or from the in situ reduction‐diazotization of nitrobenzene derivatives. The in situ diazotization of the aniline, directly or from
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Biomimetic Orthogonal Removal of Arylacyl Protecting Groups from the C-Terminus of Substituted Amino Acids and Oligopeptides via Flavin N(5)-iminium Covalent Adducts Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-02-03 Tetiana Pavlovska, Martin Havlík, Magdalena Labíková, Radek Cibulka
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Rubottom Oxidation Reaction Inspired Divergent Synthesis of α-Hydroxy Amidines, α-Bromo Amidines and Tribrominated Indole Derivatives Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-02-03 Yan-Qiu Deng, Chang-Qing Qin, Hai Ren, Guo-Shu Chen, Chen-Chen Ni, Yun-Lin Liu
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Metal-Free, Selective Ortho-Deuteration of N-Heterocyclic Oxides Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-31 Arianna Montoli, Alessandro Dimasi, Andrea Citarella, Paolo Ronchi, Daniele Passarella, Valerio Fasano
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Electrochemical Umpolung of C−H Nucleophiles Bearing Three Electron-Withdrawing Groups to Trigger Radical 1,2-Alkylarylations of Allylic Alcohols Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-31 Qibin Li, Die Hu, Kun Xu, Chengchu Zeng
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Electrochemical Oxidative Carbonylation/Coupling Reaction Using Anode to Oxidize the Trasition‐Metal‐Catalyst and Substrate Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-28 Mengyu Peng, Qingge Zhao, Longqiang Zhao, Huimin Li, Shoucai Wang, Guangbin Jiang, Fanghua Ji
We reported an electrochemical oxidative carbonylation of N‐phenylpyridin‐2‐amine derivatives under mild condtions without an external oxidant. Our approach demonstrated a novel electrochemical oxidative carbonylation reaction mode in which the simultaneous reaction of catalyst and substrate with the anode has been developed. Furthermore, an electrochemical C‐H activation for the synthesis of cyclized
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Magnesium-Mediated Reductive Defluorinative Cross-Electrophile Coupling of α-Trifluoromethyl Styrenes with CO2 and Acyl Imidazoles Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-27 Jianjun Hao, Lu Ren, Jingwen Tan, Yulin Peng, Linhai Jing, Pan Han
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Visible Light-Promoted Cascade Sulfonylation-Cyclization-Aromatization of Tertiary Enamides to Access Multi-Substituted Pyridines and 1,2-Dihydropyridines Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-27 Xin-Ming Xu, Jiping Wang, Sen Chen, Xiaoxu Chen, Jinchun Chen, Qian Liu, Zu-Li Wang, Miao Tian, Kai Sun
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Photo-Induced 3-Alkylation of Coumarins with Alkyl Halides Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-27 Cheng Yan, Wen-Jiao Zhang, Liu-Yan Qiu, Rui Wang, Weiguo Cao, Zhikun Zhang, Xiao-Jun Tang
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Data-Driven Analysis of Ni-Catalyzed Semihydrogenations of Alkynes Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-27 Miguel Martinez-Fernandez, Md Bin Yeamin, David Dalmau, Jorge J. Carbó, Albert Poater, Juan V. Alegre-Requena
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Combined Electrooxidation and Proline Catalysis for Asymmetric Formal Cross-Dehydrogenative Coupling of Benzylic Alcohols with Ketones Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-27 Hong-Ping Pu, Chao-Jiu Long, Zhe-Kai Liu, Zhi Guan, Yan-Hong He
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Synthesis of Layered Copper-Based 2D-MOFs for Enhanced Catalytic Regioselective Phosphorylation of Alkynes and P−H Bonds Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-24 Shipan Xu, Biquan Xiong, Minjing Yuan, Weifeng Xu, Renfeng Cao, Fan Cao, Longzhi Zhu, Shuang-Feng Yin
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Imidazolium-Dithiocarboxylate Zwitterions Catalysed Ring-Opening Additions of Cyclopropenones Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-22 Qi Wu, Fang Zhang, Qichao Zhang, Lin He, Jichang Liu, Guangfen Du
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γ-Terpinene: Biorenewable Reductant for the Molybdenum-Catalyzed Reduction of Sulfoxides, N-Oxides and Nitroarenes Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-21 Raquel Hernández-Ruiz, Marta Solas, Samuel Suárez-Pantiga, María R. Pedrosa, Roberto Sanz
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Base-Mediated Four-Component Intramolecular Cyclization Reaction: One-Pot Access to Imidazole-4-(2H)-Ones Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-21 Ganesh P. Pawar, Indrajeet J. Barve, Li-Ching Shen, Chung-Ming Sun
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Alkylation of Imines with Alkyl Halides under Electrochemical Conditions Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-21 Tan Zhang, Mengyun Wu, Wenhui Wang, Yingsibing Fan, Ping Liu, Peipei Sun
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CORRIGENDUM: Corrigendum to “Heterogeneous Bifunctional Catalytic, Chemo-, Regio- and Enantioselective Cascade Inverse Electron Demand Diels–Alder Reaction” Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-21 Hao Zhu
The caption of Figure 1 is incorrect. The caption should have read: “Figure 1. TEM images of a) Fe3O4 magnetic nanoparticles (10 nm), b) MNPs-supported catalyst 1 e (50 nm), c) MNPs-supported catalyst 1 e (100 nm), d) 1e after recycling ten times, e) MNPs-supported catalyst 1 g, f) MNPs (200 nm)-supported catalyst 1 f.“ As a result, the description of Figure 1 should have read: “The TEM images indicated
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Brønsted Acid-Catalyzed Enantioselective and Para-Selective Addition of Phenols to 1-Alkynylnaphth-2-Ols Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-21 Anjali Dahiya, Kalyan Dhara, Jordan Garo, Julien Gicquiaud, Alexandre Karnat, Murielle Berlande, Philippe Hermange, Jean-Marc Sotiropoulos, Patrick Y. Toullec
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Co(III)-Catalyzed Regioselective C−H Dienylation of Indolines and Indoles with Allenyl Carbinol Acetates Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-21 Rahul K. Shukla, Anurag Singh, Rakesh Shetty, Chandra M. R. Volla
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Scalable Electrochemical Dehalogenative Carboxylation without a Sacrificial Metal Anode Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-21 Nikola Petrovic, Gabriele Laudadio, Chase A. Salazar, Caleb J. Kong, Jenson Verghese, Alexander Hesketh, Giselle P. Reyes, Jean-Nicolas Desrosiers, C. Oliver Kappe, David Cantillo
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The Latest Insights into Multiply Selective Diels–Alder Reactions Using a Chiral-Cavity-Structured Lewis-Acidic Boron Catalyst Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-21 Kai Matsui, Kohei Toh, Tatsuhiro Sakamoto, Manabu Hatano, Kazuaki Ishihara
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Visible-Light-Promoted Photocatalyst-Free Unsymmetrical Synthesis of Diaryl 1, 2-Diketones from Terminal Alkynes/ Alkenes and Aryl Halides Under the Formate-Air-DMSO Condition Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-21 Xueqin Chen, Xiaoqing Wen, Yang Fu, Yingtian Liu, Rui Tan, Jiahong Li
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Dual HATs‐mediated Catalyst‐free sp3 C‐H Bond Functionalization for Regioselective Radical Hydroalkylation of Ynazoles Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-21 Yu-Xin Wu, Xiang Chen, Bang-Yan Ou, Qian Yan, Si-Han Chen, Ya-Wen Zhao, Zhi-Wei Li, Han-Wen Liu, Jiang-Sheng Li
Direct hydroalkylation of ynazoles, facilitating the efficient synthesis of linear N‐β‐vinylazoles, is accomplished through the functionalization of sp3 C‐H bonds using trace amounts of dioxygen as an initiator. This reagent‐free method eliminates the need for exogenous reagents and proceeds through a radical chain mechanism involving dual hydrogen atom transfer (HAT) processes. Its application potential
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Regio‐ and Stereoselective β‐C(sp3)‒H Activation/ Functionalization of Saturated Nitrogen Heterocycles, Amines and Amides Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-21 Sanjay Yadav, Murugesh V, Surisetti Suresh
Regio‐ and stereoselective β‐C(sp3)‒H bond functionalizations of saturated nitrogen heterocycles, amines/amides are challenging and have emerged as an important topic of research in the area of C(sp3)‒H activation. Herein, we have summarized various β‐C(sp3)‒H activation/functionalization methods; this review provides an overview of various trending approaches for β‐C(sp3)‒H bond activation/functionalization
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NFSI-TEMPO Catalysed Stereoselective Synthesis of 2-Deoxyglycosides from Glycals Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-20 Vivek Kumar Sharma, Rima Thakur
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Organic Photoredox Catalytic Sulfonylation of Enaminones to Access 3-Sulfonyl Chromones Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-16 Jun Sun, Yu Wei, Wenjian Wang, Wen Lin, Chaodong Wang, Jiadi Zhou, Guan Wang, Jianjun Li
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Catalyst-Free Sequential Wolff Rearrangement and [3+3] Annulation of Enaminones and Diazo Compounds Enabling the Assembly of Highly Functionalized Pyridin-4-Ones Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-15 Yuanzheng Wei, Longkun Chen, Huimin Hu, Yu Zhang, Shaolin Yang, Yu Xu, Li Chen, Fuchao Yu
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Controlling Catalyst Speciation to Achieve Room Temperature Pd-Catalyzed Aminations with Aryl and Heteroaryl Chlorides Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-15 Mariur Rodriguez Moreno, Mary L. Setelin, Joshua D. Hansen, James L. Corey, Kirt L. Noble, Lillian R. Stillwell, Emily Angell, Olivia A. Stubbs, Jugal Kumawat, Carlos S. Muñoz Gomez, Stacey J. Smith, Daniel H. Ess, David J. Michaelis
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1,3-Iodoesterification of 2-Substituted Indoles via Csp2−H/Csp3−H Retained Dual Functionalization Using Hypervalent Iodine(III) Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-15 Hiroko Wasaki, Katsuhiko Moriyama
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Formal [3+1+1+1] Annulation of 2-Isocyanophenyl Propargylic Esters and 4-Hydroxy-2H-Chromen-2-Ones: An Access to Quinoline-Fused Polycyclic Skeletons Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-15 Yu Xing, Xiangheng Li, Zihan Ni, Jiajian Guo, Zijun Zhou, Lei Cui, Chunju Li, Jian Li
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Iron-Catalyzed Decarboxylative and Deconstructive Cross-Coupling of Acrylic Acids with Ketone-Derived Dihydroquinazolinones Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-14 Xiao-Yu Lu, Meng-Xue Su, Hua-Yi Huang, Yu-Jun Qian, Hai-Lun Sun, Xiang Li, Xin-Ru Hu, Hao-Yu Dong
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Mg(SPh)2 as a Catalyst for Efficient Photocatalytic Alkylation Reactions of Active Methylene Compounds with Nonactivated Alkenes Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-14 Yasuhiro Yamashita, Tomoya Hisada, Yuki Sato, Shū Kobayashi
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Intramolecular Crossed [2+2] Cycloaddition through Visible-Light Triplet Sensitization: Expedient Access to Bridged Bicyclic Alkene Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-14 Min Li, Le-Yi Tao, Xin-Tao Gu, Yin Wei, Min Shi
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Photoinduced Catalytic Alkylation of Active Methine Compounds with Nonactivated Alkenes Using Yttrium Triflate as a Lewis Acid Catalyst Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-14 Yasuhiro Yamashita, Rentaro Enokijima, Yoshihiro Ogasawara, Tomoya Hisada, Shū Kobayashi
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Au(I)-Catalyzed Regiodivergent Hydroarylation of Allenes for the Synthesis of Tetrahydrodiazepines or Tetrahydrodiazonines Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-14 Pengyu Zhou, Pascal Retailleau, Vincent Gandon, Arnaud Voituriez, Xavier Guinchard
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Iron-Catalyzed Reductive Deoxygenation of Nitroarenes to Access N-Heterocycles Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-13 Ziyi Lin, Ruichen Zhang, Hong Huang, Bohao Guo, Pengjie Xian, Chang Qiao, Zhang Feng
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2-Aminoindoles and 2-Iminoindolines as Viable Precursors of Indole-Fused Nitrogenated Polyheterocycles Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-12 Alessandro Palmieri, Marino Petrini
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Regio- and Diastereoselective Cascade Synthesis of 5-Alkylidene-γ-Lactams via Copper-Catalyzed Hydro-Oxycarbonylation Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-10 Galder Llorente, Maria Teresa Herrero, Garazi Urgoitia, Raul SanMartin
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Divergent Hydroelementation of Unsaturated C−C Bonds Using 3d Transition Metal Based Catalysts Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-10 Gargi Chakraborty, Soumitra Maity
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Selective Synthesis of 2-(Indol-3-Yl)Phenols via Iodine-Catalyzed C3-Arylation of Indoles with Cyclohexanones Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-10 Qi Yin, Xinlin Zhou, Chao Zhang, Shanping Chen, Yuxia Li, Guo-Jun Deng
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Organophotocatalytic Site-Selective Radical Deuteration at Sterically Hindered Benzylic Positions by Consecutive Hydrogen Atom Transfer Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-10 Chuan-Hua Qu, Shan-Shan Chen, Lin Zhu, Yan Tang, Si-Si Zhang, Hong-Bo Peng, Gui-Ting Song
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First Bromide-Catalyzed Selenylation of 2-Alkyn-1-One O-Methyloximes Enabled the Synthesis of 4-Selenylated Isoxazoles Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-10 Jinhui Cai, Zhouting Zeng
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Synthesis of 3-Organoselenyl Quinolines through the Reduction of Alkynes Mediated by Electrophilic Organoselenium Compounds Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-09 Guilherme Lutz, Fabíola Caldeira dos Santos, Davi Fernando Back, Marcela C. Felix, Victor M. Deflon, Cristina Wayne Nogueira, Gilson Zeni
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Enzymatic Asymmetric Synthesis of All Stereoisomers of Aliphatic, Vicinal Diols in Conventional and Non-Conventional Media Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-09 Maria Nicolas, Jan-Dirk Küsters-Spöring, Chiara Aufderheide, Helen Traving, Carina Ronja Kipp, Victoria S. Pfennig, Carsten Bolm, Petra Siegert, Dörte Rother
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Copper-Mediated C−C Coupling of Alkenyl Boronates and Bromodifluoroacetates Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-09 Yevhen Yurov, Kamila Laniush, Oleksandr V. Hryschuk, Oleksandr S. Liashuk, Oleksandr O. Grygorenko
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Disclosing the Intra-Catalyst Non-Covalent Interactions in Tetrahydropyran-Based Dipeptidic Catalysts Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-08 Irma García-Monzón, Jorge Borges-González, Ezequiel Q. Morales, Israel Fernández, Tomás Martín
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Research Progress on Organocatalytic Asymmetric Synthesis of Atropisomeric Aldehydes Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-08 Xing-Xing Liu, Zi-Rou Hu, Ming-Fei Duan, Dao-Juan Cheng
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Preparation of Mesoporous Cu2O Nanospheres for Green Synthesis in the Enantioselective Boron Conjugate Addition of α,β-Unsaturated Chiral Compounds in Aqueous Phase Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-08 Xuhong Zhao, Lian Ma, Meng Wang, Weishuang Li, Yaoyao Zhang, Bojie Li, Zhongpu Fang, Bo Xiong, Lei Zhu
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Palladium-Catalyzed Cyclization Amination of Propargylamine and 1,3-Dienes Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-08 Biao Yao, Wenfang Xiong, Wanqing Wu, Huanfeng Jiang
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Visible-Light-Induced Difluoroalkylation of C(sp3)−H Bonds with Trimethylsilyl Chloride as a Dual-Function Reagent Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-01-08 Xiaochen Wang, Senhui Wu, Pengxuan Ding, Yuxiu Liu, Hongjian Song, Qingmin Wang