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Enzymatic Synthesis of Enantiopure (R)‐Citronellal from Geraniol via a Short‐Chain Dehydrogenase and Ene Reductase Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-20 Claudia Ferrer‐Carbonell, Rocio Villa, Iris Viskaal, Diederik J. Opperman, Caroline E. Paul
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Direct Site‐Selective Deoxygenation of Benzylalcohol Derivatives Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-19 Satoshi Yagi, Kazuhiro Morisaki, Yoshihiro Sato
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Integrating Visible‐Light Photocatalysis and Enzymes for the Stereoselective Synthesis of Alcohols and Amines Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-19 Stefano Parisotto, Cristina Prandi
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Catalytic Diastereoselective Synthesis of Bicyclo[3.2.1]octanediones Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-16 Liyuan Zhou, Lili Zhao, Caiyi Ren, Qinqin Cui, Shouang Lan, Chao Xu, Wennan Dong, Chunyun Jiang, Xiangwen Kong, Benlong Luo, Shuang Yang, Xinqiang Fang
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Visible Light and Hypervalent Iodine-Induced C(sp2)?H Difunctionalization: Metal-Free Dual Synthetic Approach for Carboaminated Naphthoquinones Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-16 Satyajit Pal, Subhankar Sarkar, Tanmay Pramanik, Anindita Mukherjee, Sougata Santra, Adinath Majee
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Electrochemical Chemo‐ and Regioselective Heterofunctionalization of Tropones via C(sp2)H Derivatization Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-18 Mauro Garbini, Samuele Moncullo, Sofia Kiriakidi, Manuela Melucci, Sara Bellini, Chiara Zanardi, Carlos Silva López, Giulio Bertuzzi, Marco Bandini
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Borane‐Catalyzed Chemo‐ and Regioselective Ring Opening of 2‐Substituted Aziridines with Phenols for Direct Synthesis of β‐Arylethylamines Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-18 Sanjukta Saha, Debraj Ghosh, Devendra Kumar Dhaked, Murali Mohan Guru
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Noncovalent‐Interaction‐Dictated Product Selectivity in Intermolecular and Intramolecular Controllable Oxidation of Aromatic Amines Using 2,2′‐Diperoxyphenic Acid Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-18 Liting Wang, Jingru Yin, Shaoyan Gan, Xihui Yang, Siyuan Hao, Lei Shi
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Electrochemically Driven Hydroxy‐Thiocarbamation of Electron‐Deficient Alkenes Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-18 Yu‐Fang Tan, Lan‐Xi Zong, Zhi Guan, Yan‐Hong He
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Cu/Ru Sequential Catalysis via In Situ Directing Group Formation for Site‐Selective CH Arylation Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-18 Yu‐Yong Luan, Jin‐Ye Li, Xiao‐Ping Gong, Xue‐Yuan Liu, Yong‐Min Liang
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Solvent‐ and Transition Metal‐Free Mechanochemical Synthesis of 2‐Thiazolines and S‐Thiocarbamates Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-17 Kamil Hanek, Natalia Pietras, Dawid Frąckowiak, Patrycja Żak
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Electrochemically Driven Diastereoselective Dearomative 2,3‐Diesterification of Indoles with Carboxylic Acids Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-17 Wei Zhou, Peng Chen, Xiao‐Qing Xie, Yanli Wu, Haixin Ding, Xian‐Rong Song, Ruchun Yang, Mu‐Jia Luo, Qiang Xiao
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Visible Light‐Driven Iron‐Catalyzed Decarboxylative Cyclization Reaction for Synthesis of 3‐Amino‐2,3‐Dihydrobenzofuran Derivatives from 2‐Carboxymethoxybenzaldehydes and Aryl Amines Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-16 Wenli Sheng, Zhenyu Jiang, Qingyan Liu, Junmin Chen
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Visible Light‐Promoted Esterification of Carboxylic Acids via Photoacid Generation Catalysis Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-16 Valentina Benazzi, Periklis X. Kolagkis, Lorenzo di Terlizzi, Eirini M. Galathri, Olga G. Mountanea, Maurizio Fagnoni, Stefano Protti, Christoforos G. Kokotos
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Copper‐Catalyzed Coupling Reaction of Diazo Reagent with Formamide for the Synthesis of α‐Formyloxy Ketones and α‐Ketoamides Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-16 Rongxiang Chen, Jutuan Xiao, Jing Cao, Mingli Zhu, Kai‐Kai Wang, Shouhu Li, Lantao Liu
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Insights into Alkene Hydroselenation Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-16 Hong‐Shuang Li, Shi‐Chao Lu
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Synergistic Visible Light Nanophotocatalysis and Asymmetric Organocatalysis for the Stereoselective α‐Alkylation of Aldehydes Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-16 Antonio Di Sabato, Marta Santoni, Vyali Georgian Moldoveanu, Alessandro Camilli, Marta Feroci, Giorgio Olivo, Beatrice Simonis, Elisa Sturabotti, Francesca Leonelli, Fabrizio Vetica
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Dual Photoredox/Cu‐Catalysis Enables Diastereoselective Synthesis of 3‐β‐Ethynyltropanes via Decarboxylative Alkynylation Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-16 Mayssa Zayene, Franck Le Bideau, Pascal Retailleau, Hichem Ben Jannet, Vincent Gandon, Anis Romdhane, Samir Messaoudi
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Multiphoton Multicomponent Reactions: Discovery of the 2‐Photon Ketene 4‐Component Reaction (2P‐K‐4CR) Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-16 Federica Minuto, Martina Buccioli, Pietro Capurro, Barbara Benedetti, Pavlo Solokha, Serena De Negri, Davide Ravelli, Andrea Basso
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Electrosynthesis of 2,5‐Disubstituted Furans through a CC Double Bond Cleavage Radical Cascade Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-16 Xinhao Fan, Chengcheng Yuan, Chengkou Liu, Lianhui Chen, Xi Yang, Linjingran Chen, Zefu Zheng, Zheng Fang, Kai Guo
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B(C6F5)3‐Catalyzed Reductive CC Bond Cleavage of Bisindolylmethanes Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-13 Kaibo Xu, Zhenguo Zhang, Bohan Li, Jinling Li, Teck‐Peng Loh, Zhenhua Jia
In this study, B(C6F5)3‐catalyzed reductive CC bond cleavage of bisindolylmethanes (BIMs) is reported as an efficient strategy for preparing C3‐alkylated indoles. In the presence of silane, B(C6F5)3 selectively activates Csp2‐Csp3 bonds of BIMs under mild conditions. Moreover, this sustainable process exhibits a broad substrate scope, highly functional group tolerance, and excellent regioselectivity
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Concise Synthesis of Carbocycle‐Fused γ‐Carbolinones via Regio‐/Chemoselective Reaction of Indole‐3‐Carboxamides with Cyclic Diazo Compounds Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-13 Chang Gao, Bin Li, Biao Cheng, Qianting Zhou, Xinying Zhang, Xuesen Fan
γ‐Carboline and γ‐carbolinone are privileged structural scaffolds for the development of new pharmaceuticals and functional materials. A concise and effective synthesis of carbocycle‐fused γ‐carbolinone derivatives via the regio‐ and chemoselective cascade reactions of indole‐3‐carboxamides with cyclic diazo compounds is presented. The formation of product is initiated by the regioselective C2H bond
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eAmidation: An Electrochemical Amidation of Aldehydes via the Oxidation of N‐Aryl Hydrazones Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-13 Luke Chen, James David Francis Thompson, Craig Jamieson
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Visible Light-Driven Photoredox Synthesis of Sulfonylated Benzimidazoisoquinolines via 10 H-Phenothiazine-Catalyzed Electron Donor–Acceptor Complexes Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-12 Zhi-Xing Liu, Yi Lv, Na-Zi Li, Zi-Rui Kuang, Lan-Yan He, Cheng-Liang Liu, Chen-Xi Zhang, Zhi-Wei Li, Han-Wen Liu, Jiang-Sheng Li
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Electrochemical Oxidative [3 + 2] Annulation of p-Methoxy Anilines with Enaminones toward 3-Acyl Indoles Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-12 Luchao Li, Pei Guan, Yongfang Wang, Longyu Deng, Caipeng Wang, Delong Ma, Yan Meng, Zheng Fang, Jindian Duan, Kai Guo
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Impact of the Substitution Pattern in N–heterocyclic Olefin‐Substituted Phosphines on Palladium Catalysis Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-12 Nicolas Kaiser, Aya Alhaddad, Julian Löffler, Viktoria H. Gessner
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Metal‐Free Nitration/Cyclization of Unactivated Olefins to Access Nitroated Tetrahydropyridazines with Sodium Nitrate Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-12 Xian Liu, Liqiang Hao, Xiao Yu, Shengkui Jin, Yiping Liu, Yafei Ji
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C–H Homocoupling of Arenes via Pd/S,O‐Ligand Catalysis Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-12 Ke‐Zuan Deng, Sam Pikavet, Paola Riente, María Ángeles Fernández‐Ibáñez
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Bifunctional Reagents for Photochemical Synthesis Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-12 Jia‐Yao Feng, Ming‐Qi Yang, Hong‐Lin Wu, Ying Tong, Xi‐Ni Luo, Shi‐Qing Zhang, Rong‐Nan Yi, Jun‐Qi Zhang, Yi‐Ping Ruan, Wen‐Ting Wei
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Front Cover Picture: High‐Performance and Recyclable Multisite Catalytic System for CO2 Fixation Using Crown Ether‐Linked Schiff Base and Alkali Halides (Adv. Synth. Catal. 11/2025) Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-11 Md. Saddam Hossain, Yu Hoshino, Hisashi Shimakoshi
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High‐Order Cascade Transformations on Tertiary β‐Enaminones for Step‐Economical Construction of Molecular Diversity and Complexity Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-10 Chenxu Wang, Jianchao Liu, Jie‐Ping Wan
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Total Synthesis of (−)‐2‐Oxokolavenol: A Natural Neoclerodane Diterpene with Farnesoid X Receptor Transcriptional Activity Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-10 Da‐Yu Shi, Wen‐Bo Ye, Rui Ding, Ding‐Ding Gao, Yi‐Wen Zhao, Cheng Huang, Ping Tian
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Pd‐Catalyzed Regio‐ and Stereoselective Ring‐Opening Hydrosulfonylation of Methylenecyclopropanes for Branched Allylic Sulfones Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-06-09 Bu‐Hong Zhang, Jia‐Xin Song, Bai‐Lin Wang, Zhi‐Xiong Ou, Li‐Bo Li, Xing‐Wang Wang
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Synthesis of spirolactones from carbonyls via carboborylation of N‐sulfonylhydrazones with alkoxycarbonylalkylboronic acids Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-26 Lucía López, Sara Filgueira, María-Paz Cabal, Alfonso Carlos Valdés-Gómez
A straightforward synthesis of spirolactones from carbonyls via N‐tosylhydrazones is described. The process consist in the reaction between the N‐tosylhydrazone and ethoxycarbonylethylboronic acid or ethoxycarbonylpropylboronic acid, leading to spiro γ‐butyrolactones or δ‐valerolactones respectively. The transformation takes place by carboborylation of the N‐tosylhydrazone followed by oxidation of
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Transition Metal-Catalyzed Directing Group-Assisted Site-Selective Di-Ortho C?H Functionalizations via Double C?H Activation Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-25 Swadhin Swaraj Acharya, Padma Ranjan Rout, Rudranarayan Sutar, Chiranjib Pradhan, Bibhuti Bhusan Parida
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Oxidative Rearrangement of 3-Aryl Azo Indoles in Water: Synthesis of C3-Oxo-C2-Amino Indoles and their Application as Fluorophores for Lipid Droplet Detection Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-25 Tejas Prabakar, Payal Ambastha, Rashmi Yadav, Animesh Samanta, Mahesh Kumar Ravva, Parthapratim Munshi, Subhabrata Sen
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Skeletal Editing of 6-(Hetero)arenes via Single-Carbon-Atom Insertion Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-24 Xuheng Zhang, Yuanhao Zhu, Wei Jiang, Zhengyu Zhang, Yaojia Jiang
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Dearomative, Intramolecular Bromoetherification of Carbohydrate‐derived Glycosyl Furans: Access to Enantiopure 6‐Bromo‐Furo[3,2‐b]furans Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-24 William J. Berkey, Lindsey R. C. Bryson, Russell Kirkland, Kaitlyn S. Otte, Christopher W. Jones, Stefan France
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Synthesis and Applications of 9/9,9-Substituted Fluorene Derivatives Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-23 Chao Liu, Ying Wei, Linghai Xie
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Visible-Light Induced Cyclization to Carbazole-Fused Eight-Membered Diazocan-5-ones Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-22 Feng Zhao, Fei Liu, Tongtong Shi, Ting Sun, Lianglong Sun, Si Chen, Xin Wang, Kai Sun
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Asymmetric Synthesis of Highly Substituted Spiro[2H-pyrrole-2,3-Succinimide] Derivatives by Copper-Catalyzed Post-Ugi Reactions Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-22 Javier Gómez-Ayuso, Israel Carreira-Barral, Roberto Quesada, María García-Valverde
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Cobalt-Catalyzed Enantioselective Alkenylative Cyclization of 1,6-Allenynes† Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-17 Tao Wang, Ji-Xun Guan, Yun-Xuan Tan, Ping Tian
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Development of Hydrofluoroolefin (HFO)-Based Direct O-Fluoroalkenylation of Phenols Targeting Tyrosine Conjugation Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-17 Rihárd Sisa, Ferenc Béke, Zoltán Novák
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Recent Advances in Annulation Reactions of α,β-Unsaturated Ketoximes for the Synthesis of Structurally Diversified Heterocycles Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-17 Gaochen Xu, Yongfang Wang, Yan Meng, Zheng Fang, Jindian Duan, Kai Guo
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Chemoselective Synthesis of α‐Chloro and α,α ‐Dichloro acetamidines via the Carbenoids Addition to Inherently Low Electrophilic Carbodiimides Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-17 Davide Castiglione, Margherita Miele, Alberto Nardi, Laura Castoldi, Vittorio Pace
The hitherto few explored α‐halomethyl amidine motif has been assembled through the addition of a lithiated (di)‐halomethane (i.e. carbenoid) to easily accessible N,N’‐diaryl substituted carbodiimides. Despite the inherent low electrophilicity of these heterocumulenes – as quantitatively determined in Mayr’s previous studies – their sp‐hybridized carbon atom acts as a competent site of attack for these
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Metal‐Free Divergent Photocatalytic Cascade [4+2] Addition‐Defluorinative Annulation of gem‐Difluoroalkenes with Terminal Alkynes Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-17 Dong‐Sheng Li, Guang‐Xu Zhang, Hao Qian, Fei Xue, Hong‐Ping Deng
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Synthesis of Polysubstituted Naphthalenes via Metal‐Free Borylative Cyclization of o‐Alkynylstyrenes Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-15 Marcos Humanes, Manuel A. Fernández‐Rodríguez, Patricia García‐García
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Pot‐Economical Synthesis of Fluorinated Pyrrolizinone Derivatives Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-15 Lidia Prieto, Marcos Escolano, Daniel Gaviña, Luis Paredes‐Soler, Santiago Díaz‐Oltra, María Sánchez‐Roselló, Carlos del Pozo
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Homogeneous Copper‐Catalyzed Cycloisomerization Reaction of Allenynes: Rapid Access to Functionalized Pyrroles Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-15 Kua‐Fei Wei, Xiu‐Hong Zhu, Guang‐Xin Ru, Wen‐Bo Shen
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Illuminating the Path of Rearrangement: Visible Light‐Driven Pd‐Catalyzed Substituted Olefins Synthesis Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-15 Jenifer Sharshonov, Valentin Duchemann, Yuqian Sun, Christine Tran, Philippe Belmont, Abdallah Hamze, Diana Lamaa, Etienne Brachet
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Sustainable Synthesis of Quinazolinones Through Boiler Flue Gas CO2 Utilization Via Pd@POP‐1 Catalyst Under Mild Conditions Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-11 Ying Liang, Kai‐Zhi Xu, Pei‐Bo Chen, Ping Fang, Jian Huang, Ying‐Ming Pan
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eAmidation: An Electrochemical Amidation of Aldehydes via the Oxidation of N‐Aryl Hydrazones Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-11 Luke Chen, James Thompson, Craig Jamieson
In recent years, the use of electrochemistry has emerged as a powerful yet sustainable means of enabling key transformations. Amidation is one of the most frequently executed transformations in synthetic chemistry, and using an electrochemical approach, the current study has demonstrated the synthesis of amides from aldehydes and amines. Mechanistic work indicates that the reaction proceeds via the
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Harnessing Nitroarenes in Streamlined Synthesis of 4‐Quinolones via Reductive C−N Coupling Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-11 Ni Dong, Xiao‐Tian Zhang, Qin Tang, Jia‐Xin Qian, Qi‐Qi Luo, Long Cheng, Tian Cao, Xiang‐Wei Liu
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Regio‐, Stereoselective, Aerobic and Metal‐Free Synthesis of Z‐Vinyl Sulfides: One‐Pot Hydroiodination of Internal Alkynes and in situ Sulfenylations Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-11 Gloria Morís‐Menéndez, Sergio E. García‐Garrido, Pablo García‐Álvarez, Alejandro Presa Soto, Nicolás Ríos‐Lombardía, Joaquín García‐Álvarez
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High-Performance and Recyclable Multisite Catalytic System for CO2 Fixation Using Crown Ether-Linked Schiff Base and Alkali Halides Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-10 Md. Saddam Hossain, Yu Hoshino, Hisashi Shimakoshi
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Development of Photo‐Biocatalytic Redox System for Asymmetric Synthesis of Optically Active Amines Using Blue Light and Transaminases. A Case Study Toward Mavacamten Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-10 Natalia Antos, Aleksandra Rudzka, Anna Hoser, Tamara Reiter, Wolfgang Kroutil, Paweł Borowiecki
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Titanium Catalyzed the Cross-Coupling of Nitriles and Alkyl Halides for the Synthesis of Ketones Adv. Synth. Catal. (IF 4.4) Pub Date : 2025-04-10 Fanxiang Zeng, Biao Ma, Yiru Wang, Haocong Li, Minghui Zhang, Zhanyu Li