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Photocatalytic Obtaining and Optical Properties of Composites Based on Layered Niobates and Silver Nanoparticles
Theoretical and Experimental Chemistry ( IF 0.7 ) Pub Date : 2022-06-01 , DOI: 10.1007/s11237-022-09719-4
V. V. Shvalagin , G. Ya. Grodzyuk , S. Ya. Kuchmiy , M. A. Skoryk

The photocatalytic properties of layered semiconductors, namely KNb3O8, and a product of its acid treatment, namely K3H3Nb10.8O30 in the reduction reaction of silver ions with the formation of the corresponding metal-semiconductor nanostructures are established. Electron microscopy has shown that silver nanoparticles are deposited mainly on the edges of niobate rods and plates when potassium niobate suspensions are irradiated with UV light in the presence of AgNO3. Silver nanoparticles of 10-30 nm are formed when K3H3Nb10.8O30 is used as a photocatalyst; they are deposited on the niobate surface and practically do not have a surface plasmon resonance band in the visible range of the spectrum, which may be associated with the formation of Ag2O on the surface of silver nanoparticles or the formation of their chain aggregates.



中文翻译:

基于层状铌酸盐和银纳米粒子的复合材料的光催化获得和光学性能

建立了层状半导体KNb 3 O 8及其酸处理产物K 3 H 3 Nb 10.8 O 30在银离子还原反应中形成相应的金属-半导体纳米结构的光催化性能。电子显微镜表明,当在 AgNO 3存在下用紫外线照射铌酸钾悬浮液时,银纳米颗粒主要沉积在铌酸盐棒和板的边缘。当K 3 H 3 Nb 10.8 O 30形成10-30 nm的银纳米粒子用作光催化剂;它们沉积在铌酸盐表面,实际上在可见光谱范围内没有表面等离子共振带,这可能与银纳米粒子表面Ag 2 O 的形成或其链状聚集体的形成有关。

更新日期:2022-06-02
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