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Enhanced Photocatalytic and Biological Observations of Green Synthesized Activated Carbon, Activated Carbon Doped Silver and Activated Carbon/Silver/Titanium Dioxide Nanocomposites
Journal of Inorganic and Organometallic Polymers and Materials ( IF 3.9 ) Pub Date : 2021-09-02 , DOI: 10.1007/s10904-021-02096-w
M. Aravind 1 , M. Amalanathan 1 , M. Sony Michael Mary 2 , C. Parvathiraja 3 , Asma A. Alothman 4 , Saikh M. Wabaidur 4 , Mohammad Ataul Islam 5
Affiliation  

In this study, Activated carbon/Silver/Titanium dioxide nanocomposite was successfully synthesized by hydrothermal method using jasmine flower extract. The reactions of reduction, stabilization and capping were executed from the biomolecules of jasmine flower extract. The decoration of activated carbon and noble metal to the metal oxide enhanced the properties in all ways. As the modified structural, optical and morphological properties of as-prepared nanocomposite were characterized using various techniques such as X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), UV–visible spectroscopy, Scanning electron microscope (SEM) with Energy dispersive X-ray spectroscopy (EDX), and Transmission electron microscope (TEM). The photocatalytic activities under sunlight were evaluated by the degradation of methylene blue (MB). Antibacterial activity was tested against E. coli and S. aureus. The characterization results show that the Activated carbon/Silver/Titanium dioxide nanocomposite is crystalline, needle like morphology and highly optically active catalyst. The investigated Activated carbon/Silver/Titanium dioxide nanocomposite shows 96% maximum degradation efficiency at the end of 120 min under visible light irradiation. The degradation efficiency and antibacterial activity are readily higher than that of commercial TiO2. The plasmonic support to the activated carbon and titanium nanoparticles creates a large surface area, active sites and accelerated the free radical generation. These characteristics demonstrated that the prepared Activated carbon/Silver/Titanium dioxide nanocomposite material is highly suitable for the decomposition of methylene blue and wastewater treatment.



中文翻译:

绿色合成活性炭、活性炭掺杂银和活性炭/银/二氧化钛纳米复合材料的增强光催化和生物学观察

本研究以茉莉花提取物为原料,通过水热法成功合成了活性炭/银/二氧化钛纳米复合材料。茉莉花提取物的生物分子进行还原、稳定和加帽反应。活性炭和贵金属对金属氧化物的装饰在各方面增强了性能。由于使用 X 射线衍射 (XRD)、傅里叶变换红外光谱 (FTIR)、紫外-可见光谱、具有能量的扫描电子显微镜 (SEM) 等各种技术对制备的纳米复合材料的改性结构、光学和形态特性进行了表征。色散 X 射线光谱 (EDX) 和透射电子显微镜 (TEM)。阳光下的光催化活性通过亚甲基蓝(MB)的降解来评估。大肠杆菌金黄色葡萄球菌。表征结果表明,活性炭/银/二氧化钛纳米复合材料是结晶、针状形态和高光学活性的催化剂。所研究的活性炭/银/二氧化钛纳米复合材料在可见光照射下 120 分钟结束时显示出 96% 的最大降解效率。降解效率和抗菌活性明显高于商用TiO 2. 对活性炭和钛纳米颗粒的等离子体支持产生了大的表面积、活性位点并加速了自由基的产生。这些特性表明所制备的活性炭/银/二氧化钛纳米复合材料非常适用于亚甲基蓝的分解和废水处理。

更新日期:2021-09-04
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