Er³⁺–Yb³⁺–Mo⁶⁺ co-doped TiO₂/Yb₂Ti₂O₇ up-conversion luminescent nanofibers have been successfully synthesized using the electrospinning technology followed by thermolysis. The effects of the precursor ratio and annealing process on up-conversion luminescent character were investigated. The phase of TiO₂ was determined to be either anatase or rutile. And the cubic Yb₂Ti₂O₇ in Er³⁺–Yb³⁺–Mo⁶⁺ co-doped TiO₂ phosphor was confirmed. After annealing at high temperature, the up-conversion luminescent intensity of the studied system increased obviously. The fluorescence intensity ratio (FIR) used to be made on the basis of green up-conversion emissions. It was studied as a function of temperature. The maximum rate of sensitivity was ~0.01 K⁻¹ in the range of 300–600 K. The results indicate that Er³⁺–Yb³⁺–Mo⁶⁺ co-doped TiO₂/Yb₂Ti₂O₇ phosphor is a brand-new material that meets the requirement of the optical temperature sensing.

尔³⁺ -Yb ³⁺ -Mo ⁶⁺共掺杂的TiO ₂的Yb / ₂的Ti ₂ ö ₇上转换发光纳米纤维利用静电纺丝技术成功地合成，随后通过热。研究了前驱体比例和退火工艺对上转换发光特性的影响。TiO ₂的相被确定为锐钛矿或金红石。和立方晶的Yb ₂的Ti ₂ ö ₇在铒³⁺ -Yb ³⁺ -Mo ⁶⁺共掺杂的TiO ₂磷被证实。高温退火后，所研究体系的上转换发光强度明显增加。荧光强度比 (FIR) 过去是基于绿色上转换发射得出的。它被研究为温度的函数。灵敏度的最大值率为〜0.01ķ ^-1在300-600 K的范围的结果表明，二³⁺ -Yb ³⁺ -Mo ⁶⁺共掺杂的TiO ₂ /镱₂的Ti ₂ ö ₇磷光体是满足光学温度传感要求的全新材料。