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ZS-1 Zeolite as a Highly Efficient and Reusable Catalyst for Facile Synthesis of 1-amidoalkyl-2-naphthols Under Solvent-Free Conditions
Catalysis Letters ( IF 2.3 ) Pub Date : 2021-06-04 , DOI: 10.1007/s10562-021-03684-8
Sudarshan S. Dipake , Sachin P. Gadekar , Premkumar B. Thombre , Machhindra K. Lande , Anjali S. Rajbhoj , Suresh T. Gaikwad

Efficient and reusable ZS-1 zeolite as a novel catalyst was successfully synthesized by the hydrothermal method. Characterizations of catalysts were carried out using diverse analysis techniques such as XRD, FT-IR, FESEM, EDAX, HRTEM, BET, and NH3TPD. Promoted as an environment-friendly protocol for the facile synthesis of various substituted 1-amidoalkyl-2-naphthols through the reaction of β-naphthol, aldehyde, and amides under solvent-free conditions. This catalyst provides many advantages such as shorter reaction times, operational simplicity, reusability, an excellent yield of the product, facile work-up, and easily recoverable. Moreover, the recovered catalyst can be recycled and reused for the next five runs without significant loss of catalytic activity.

Graphic Abstract



中文翻译:

ZS-1 沸石作为一种高效且可重复使用的催化剂,用于在无溶剂条件下轻松合成 1-酰胺基烷基-2-萘酚

采用水热法成功合成了高效且可重复使用的ZS-1沸石作为一种新型催化剂。催化剂的表征使用多种分析技术进行,例如 XRD、FT-IR、FESEM、EDAX、HRTEM、BET 和 NH 3 TPD。通过β-萘酚、醛和酰胺在无溶剂条件下的反应轻松合成各种取代的1-酰氨基烷基-2-萘酚的环境友好型方案。这种催化剂具有许多优点,例如反应时间更短、操作简单、可重复使用、产品收率高、易于后处理和易于回收。此外,回收的催化剂可以在接下来的五次运行中循环使用,而不会显着降低催化活性。

图形摘要

更新日期:2021-06-04
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