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Fine Ultra-small Ruthenium Oxide Nanoparticle Synthesis by Using Catharanthus roseus and Moringa oleifera Leaf Extracts and Their Efficacy Towards In Vitro Assays, Antimicrobial Activity and Catalytic: Adsorption Kinetic Studies Using Methylene Blue Dye
Journal of Cluster Science ( IF 2.7 ) Pub Date : 2021-03-11 , DOI: 10.1007/s10876-021-02037-0
S. M. Anjum , K. Riazunnisa

A simple one step green procedure is intended to investigate for the first time by employing ruthenium oxide nanoparticles (RuO2 NPs) derived from Catharanthus roseus (CR) and Moringa oleifera (MO) leaves and evaluate their catalytic—degradation of MB dye, antibacterial screening and in vitro antioxidant assays. The as-synthesized RuO2 NPs were characterized by XRD, HR-TEM, FT-IR, EDX and UV–Visible spectrometer. The HR-TEM image reveals spherical morphology with average particle size 5.6 nm (CR-RuO2 NP) and 4.6 nm (MO-RuO2 NP). The research findings of the current study elucidates the superiority of CR-RuO2 NPs and well exhibited towards scavenging activity, admirable anti-bacterial effect against K. pneumonia (21.6 ± 0.24 mm), and catalytic degradation percentage as 79.02%. The adsorption kinetics indeed suggest more impressive pseudo-second-order kinetic model than Lagergren first-order kinetics at 10 ppm concentration of MB dye. Our results thus provide a platform for further research on the applications of RuO2 NPs as disinfectant and better catalyst.



中文翻译:

长春花和辣木叶片提取物合成超细氧化钌纳米粒子及其对体外测定,抗菌活性和催化作用的研究:亚甲基蓝染料的吸附动力学研究

一种简单的一步绿色程序旨在通过使用源自长春花(CR)和辣木(MO)叶片的氧化钌纳米颗粒(RuO 2 NPs)进行首次研究,并评估它们的催化降解MB染料,抗菌筛选和体外抗氧化剂测定。通过XRD,HR-TEM,FT-IR,EDX和紫外可见光谱仪对合成的RuO 2 NP进行了表征。HR-TEM图像显示出球形形态,平均粒径为5.6 nm(CR-RuO 2 NP)和4.6 nm(MO-RuO 2 NP)。本研究的研究结果阐明了CR-RuO 2的优越性NPs和NPs具有清除活性,对肺炎克雷伯菌具有令人钦佩的抗菌作用(21.6±0.24 mm),催化降解率为79.02%。实际上,在10 ppm的MB染料浓度下,吸附动力学确实比Lagergren一级动力学更令人印象深刻的伪二级动力学模型。因此,我们的结果为进一步研究RuO 2 NP作为消毒剂和更好的催化剂的应用提供了平台。

更新日期:2021-03-11
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