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Tandem Mass Spectrometry in the Technology of Determining Aralosides of Phytoadaptogene Compositions
Theoretical Foundations of Chemical Engineering ( IF 0.8 ) Pub Date : 2021-01-15 , DOI: 10.1134/s0040579520050334
I. V. Kazeev , O. A. Bocharova , V. E. Shevchenko , R. V. Karpova , E. V. Bocharov , E. V. Uyutova , O. P. Sheychenko , V. G. Kucheryan , M. A. Baryshnikova

Abstract

The possibilities of tandem mass spectrometry have been studied for the technology of analyzing aralosides in the pharmaceutical composition of Multifitoadaptogen (MFA) and extract of the roots of Aralia mandshurica (which is an ingredient in MFA). Chromatography is performed on an ACQUITY UPLC BEH C18 column in gradient mode. A TSQ Vantage electrospray ionization triple quadrupole mass spectrometer is used. In MFA, as well as in the extract of the roots of Aralia mandshurica, Aralosides A, B, C, and/or their isomers are identified.



中文翻译:

串联质谱法测定植物调节素成分的无糖苷

摘要

串联质谱法的可能性已研究了在Multifitoadaptogen(MFA)和的根的提取物的药物组合物分析龙牙葱木皂苷的技术龙牙楸(这是在一个MFA成分)。色谱法在ACQUITY UPLC BEH C18色谱柱上以梯度模式进行。使用TSQ Vantage电喷雾电离三重四极杆质谱仪。在MFA中,以及在五加木(Aralia mandshurica)的根提取物中,均鉴定出Aralosides A,B,C和/或其异构体。

更新日期:2021-01-15
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