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Synthesis, Molecular, and Crystal Structure of Tris(2-carbamoylmethoxyphenyl)phosphine Oxide
Russian Journal of General Chemistry ( IF 0.9 ) Pub Date : 2020-11-17 , DOI: 10.1134/s1070363220100059 T. V. Baulina , I. Yu. Kudryavtsev , A. V. Artem’ev , I. Yu. Bagryanskaya , M. P. Pasechnik , V. K. Brel
中文翻译:
三(2-氨基甲酰基甲氧基苯基)膦氧化物的合成,分子及晶体结构
更新日期:2020-11-17
Russian Journal of General Chemistry ( IF 0.9 ) Pub Date : 2020-11-17 , DOI: 10.1134/s1070363220100059 T. V. Baulina , I. Yu. Kudryavtsev , A. V. Artem’ev , I. Yu. Bagryanskaya , M. P. Pasechnik , V. K. Brel
Abstract
New tripodal ligand, tris(2-carbamoylmethoxyphenyl)phosphine oxide, has been synthesized via the alkylation of tris(2-hydroxyphenyl)phosphine oxide with chloroacetamide. The ligand structure has been studied by means of IR and NMR (1H, 31P) spectroscopy as well as X-ray diffraction.
中文翻译:
三(2-氨基甲酰基甲氧基苯基)膦氧化物的合成,分子及晶体结构
摘要
通过将三(2-羟苯基)膦氧化物与氯乙酰胺烷基化,合成了新的三脚架配体三(2-氨基甲酰基甲氧基苯基)膦氧化物。已经通过IR和NMR(1 H,31 P)光谱以及X射线衍射研究了配体结构。