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Supercritical CO 2 extraction of antioxidants from Paulownia elongata x fortunei leaves
Biomass Conversion and Biorefinery ( IF 3.5 ) Pub Date : 2020-09-28 , DOI: 10.1007/s13399-020-01022-3
Paula Rodríguez-Seoane , Beatriz Díaz-Reinoso , Herminia Domínguez

Paulownia wood demand is increasing, but other parts of the tree remain underused. The leaves have medicinal properties, and their processing with a clean technology was explored. Supercritical fluid extraction (SFE) was proposed for the production of extracts from Paulownia elongata x fortunei leaves. Three isotherms (35 °C, 45 °C, and 55 °C) were studied in the pressure range of 10–30 MPa to assess their influence on the extraction yield and antiradical properties. The use of ethanol as cosolvent was also evaluated. A global extraction yield of 4 g extract /100 g of leaves was obtained at 30 MPa and 45 °C using 10% ethanol (w/w) as modifier; the last fractions reached up to 0.30 g Trolox eq./g extract. Serial extractions with different concentrations of ethanol (60, 70, 80, and 96%) were performed. The global yield obtained with 70% ethanol in three stages was 32.9 g extract/100 g leaves, and the antiradical capacity of the first stage extract was equivalent to 0.4 g Trolox/g extract. Extraction kinetics was studied, and overall extraction curves were represented using Sovová’s model.



中文翻译:

超临界CO 2提取泡桐叶片的抗氧剂。

泡桐木的需求量正在增加,但树的其他部分仍未得到充分利用。叶片具有药用特性,并探索了使用清洁技术对其进行加工的方法。提出了超临界流体萃取(SFE)用于生产泡桐(Paulownia elongata x fortunei)的提取物树叶。在10–30 MPa的压力范围内研究了三个等温线(35°C,45°C和55°C),以评估它们对提取率和抗自由基性能的影响。还评估了乙醇作为助溶剂的使用。使用10%乙醇(w / w)作为改性剂,在30 MPa和45°C的条件下,获得的总提取量为4 g提取物/ 100 g叶片;最后的馏分达到0.30 g Trolox eq./g提取物。用不同浓度的乙醇(60%,70%,80%和96%)进行了连续萃取。用70%乙醇在三个阶段中获得的总产量为32.9 g提取物/ 100 g叶片,第一阶段提取物的抗自由基能力相当于0.4 g Trolox / g提取物。研究了萃取动力学,并使用Sovová模型表示了总萃取曲线。

更新日期:2020-09-28
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