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Influence of the Organic Moiety on the Tribological Properties of MoS 2 :Glycol Hybrid Nanoparticles-Based Dispersions
Tribology Letters ( IF 2.9 ) Pub Date : 2020-09-25 , DOI: 10.1007/s11249-020-01345-2
I. García , J. Galipaud , I. Kosta , H. Grande , E. Garcia-Lecina , F. Dassenoy

MoS2:glycol hybrid nanoparticles were synthetized through a polyol route. Their tribological properties when used as lubricant additives in a PAO 6 base oil were investigated using a pin-on-disk tribometer. An important friction reduction and good anti-wear performances were observed compared to the base oil and to the no modified particles. The MoS2:glycol nanoparticles were characterized by thermogravimetric analysis, transmission electron microscopy, RAMAN spectroscopy, X-ray diffraction, and Fourier transform infrared. Furthermore, the stability of the dispersion was followed by dynamic light scattering. On the other hand, Field Emission Scanning Electron Microscopy, Energy-Dispersive X-ray Spectroscopy, and X-ray Photoelectron Spectrometry analysis showed that the tribofilm formed on the wear surfaces during the friction test is at the origin of the excellent tribological performance of the MoS2 nanoparticles. In particular, it was demonstrated that the interaction of MoS2 with the organic moiety of the nanoparticles plays a key role in the friction reduction and the good anti-wear properties of the dispersions.



中文翻译:

有机部分对基于MoS 2:乙二醇杂化纳米颗粒的分散体的摩擦学性能的影响

通过多元醇路线合成了MoS 2:乙二醇混合纳米颗粒。使用销盘式摩擦计研究了它们在PAO 6基础油中用作润滑剂添加剂时的摩擦学性能。与基础油和未改性颗粒相比,观察到重要的摩擦降低和良好的抗磨性能。MoS 2:乙二醇纳米颗粒通过热重分析,透射电子显微镜,拉曼光谱,X射线衍射和傅立叶变换红外光谱进行了表征。此外,分散体的稳定性之后是动态光散射。另一方面,场发射扫描电子显微镜,能量色散X射线能谱和X射线光电子能谱分析表明,摩擦试验期间在磨损表面上形成的摩擦膜是摩擦学性能优异的起源。 MoS 2纳米颗粒。特别地,证明了MoS 2与纳米颗粒的有机部分的相互作用在分散体的摩擦降低和良好的抗磨性能中起关键作用。

更新日期:2020-09-25
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