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Effects of Li 2 CO 3 and CuO as Composite Sintering Aids on the Structure, Piezoelectric Properties, and Temperature Stability of BiFeO 3 -BaTiO 3 Ceramics
Journal of Electronic Materials ( IF 2.2 ) Pub Date : 2020-08-11 , DOI: 10.1007/s11664-020-08365-7
Shibo Guan , Huabin Yang , Guanjun Qiao , Yuanyuan Sun , Fangmei Qin , Haigang Hou

In order to reduce the sintering temperature of ceramics, the effects of binary composite sintering aids, Li2CO3 and CuO, on the sintering temperature and properties of 0.7BiFeO3-0.3BaTiO3-0.0035MnCO3 + 0.002Li2CO3 + xCuO (BF-BT-LC + xCuO) ceramics were studied by traditional solid-state sintering. The results show that the sintering liquid phase can effectively promote the sintering of BF-BT-LC + xCuO ceramics by adding a certain amount of Li2CO3 and changing the amount of CuO. The samples sintered at 930°C/2 h with 0.4 mol.% CuO get a piezoelectric constant d33 = 168 pC/N, an electromechanical coupling coefficient kp = 0.302, and a mechanical quality factor Qm = 31.207. The addition of CuO was conducive to obtaining stable BF-BT-LC + xCuO piezoelectric ceramics. We conclude that the composite sintering aids, Li2CO3 and CuO, can effectively promote the sintering of BF-BT-LC + xCuO, which is beneficial to obtain BF-BT-LC + xCuO ceramics with a wide sintering temperature range and stable properties.



中文翻译:

Li 2 CO 3和CuO作为复合烧结助剂对BiFeO 3 -BaTiO 3陶瓷的结构,压电性能和温度稳定性的影响

为了降低陶瓷的烧结温度,二元复合烧结助剂Li 2 CO 3和CuO对0.7BiFeO 3 -0.3BaTiO 3 -0.0035MnCO 3  + 0.002Li 2 CO 3  + 的烧结温度和性能的影响。通过传统的固态烧结研究了x CuO(BF-BT-LC +  x CuO)陶瓷。结果表明,烧结液相可以通过加入一定量的Li 2 CO 3来有效地促进BF-BT-LC + x CuO陶瓷的烧结。 并改变CuO的量 在930°C / 2 h下用0.4 mol。%CuO烧结的样品的压电常数d 33  = 168 pC / N,机电耦合系数k p  = 0.302,机械品质因数Q m  = 31.207。加入的CuO有利于获得稳定的BF-BT-LC +  X CuO的压电陶瓷。结论:Li 2 CO 3和CuO复合烧结助剂可以有效地促进BF-BT-LC + x CuO的烧结 ,有利于获得烧结温度范围较宽的BF-BT-LC +  x CuO陶瓷。和稳定的属性。

更新日期:2020-08-11
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