Continuous flow synthesis of 2,2′-diselenobis(benzoic acid) and derivatives,Reaction Chemistry & Engineering

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Continuous flow synthesis of 2,2′-diselenobis(benzoic acid) and derivatives
Reaction Chemistry & Engineering ( IF 3.4 ) Pub Date : 2020-02-24 , DOI: 10.1039/d0re00012d
Francesca Begini _{1,

2,

3,

4,

5} , Dorota Krasowska _{1,

2,

3,

4,

5} , Aleksandra Jasiak _{1,

2,

3,

4,

5} , Jozef Drabowicz _{1,

2,

3,

4,

5} , Claudio Santi _{6,

7,

8,

9,

10} , Luca Sancineto _{1,

2,

3,

4,

5}

Affiliation

The continuous flow synthesis of the key building block 2,2′-diselenobis(benzoic acid) (DSBA) is herein reported. Water was used as a solvent in a reaction time as short as 90 s. This provided a successful strategy for the synthesis of DSBA which was obtained in excellent yield. The optimized procedure has been extended to DSBA derivatives.

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