Continuous flow synthesis of 2,2′-diselenobis(benzoic acid) and derivatives

Francesca Begini; Dorota Krasowska; Aleksandra Jasiak; Jozef Drabowicz; Claudio Santi; Luca Sancineto

doi:10.1039/D0RE00012D

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Continuous flow synthesis of 2,2′-diselenobis(benzoic acid) and derivatives†‡

Francesca Begini,^a Dorota Krasowska,^ab Aleksandra Jasiak,^a Jozef Drabowicz,

^ac Claudio Santi^d and Luca Sancineto

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Author affiliations

* Corresponding authors

^a Division of Organic Chemistry, Centre of Molecular and Macromolecular Studies, Polish Academy of Sciences, Sienkiewicza 112, Lodz, Poland

^b Department of Green Chemistry and Technology, Faculty of Bioscience Engineering, Campus Coupure, Ghent University, Coupure Links 653, Belgium

^c Institute of Chemistry, Health and Food Sciences, Jan Dlugosz University in Czestochowa, Armii Krajowej 13/15, 42-200 Czestochowa, Poland

^d Department of Pharmaceutical Sciences, University of Perugia, Group of Catalysis, Synthesis and Organic Green Chemistry, Via del Liceo 1, 06123 Perugia, Italy
E-mail: luca.sancineto@unipg.it

Abstract

The continuous flow synthesis of the key building block 2,2′-diselenobis(benzoic acid) (DSBA) is herein reported. Water was used as a solvent in a reaction time as short as 90 s. This provided a successful strategy for the synthesis of DSBA which was obtained in excellent yield. The optimized procedure has been extended to DSBA derivatives.

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Article information

DOI: https://doi.org/10.1039/D0RE00012D
Article type: Communication
Submitted: 08 Jan 2020
Accepted: 24 Feb 2020
First published: 24 Feb 2020

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React. Chem. Eng., 2020,5, 641-644

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Continuous flow synthesis of 2,2′-diselenobis(benzoic acid) and derivatives

F. Begini, D. Krasowska, A. Jasiak, J. Drabowicz, C. Santi and L. Sancineto, React. Chem. Eng., 2020, 5, 641 DOI: 10.1039/D0RE00012D

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Reaction Chemistry & Engineering

Continuous flow synthesis of 2,2′-diselenobis(benzoic acid) and derivatives†‡

Abstract

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Continuous flow synthesis of 2,2′-diselenobis(benzoic acid) and derivatives

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