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Preparation and Characterization of a g-C 3 N 4 /LSACF Composite and Application in RhB Degradation
Journal of Inorganic and Organometallic Polymers and Materials ( IF 3.9 ) Pub Date : 2019-08-30 , DOI: 10.1007/s10904-019-01302-0
Hang Yang , Ermao Li , Boxun Zhou , Yue Wang , Pan Li , Shibin Xia

In this study, g-C3N4/Luffa sponge activated carbon fiber (LSACF) composite was prepared as a novel bio-based photocatalyst for RhB degradation. The physical and chemical properties of the materials were measured using multiple characterization methods, including scanning electronic microscopy, transmission electronic microscopy, X-ray diffraction, energy dispersive X-ray spectroscopy, Fourier transform infrared spectroscopy, UV–Vis spectrophotometry and Brunauer–Emmett–Teller. The effects of various factors, including the kind of catalyst, the dose of catalyst, the pH value, the initial concentration of RhB and the number of cycle, on RhB degradation were investigated. In addition, radical trapping tests were performed to determine the reaction mechanism of RhB degradation. The trapping test of RhB degradation showed that superoxide radicals and holes were major contributors in the degradation of RhB. The thorough results show that the g-C3N4/LSACF composite is a promising material in RhB degradation.

中文翻译:

gC 3 N 4 / LSACF复合材料的制备,表征及其在RhB降解中的应用

在这项研究中,gC 3 N 4/ Luffa海绵活性炭纤维(LSACF)复合材料被制备为新型的基于生物的RhB降解光催化剂。使用多种表征方法测量了材料的物理和化学性质,包括扫描电子显微镜,透射电子显微镜,X射线衍射,能量色散X射线光谱,傅里叶变换红外光谱,UV-Vis分光光度法和Brunauer-Emmett-出纳员。研究了催化剂种类,催化剂用量,pH值,RhB初始浓度和循环次数等因素对RhB降解的影响。此外,进行自由基捕获测试以确定RhB降解的反应机理。RhB降解的捕获测试表明,超氧自由基和空穴是RhB降解的主要因素。彻底的结果表明gC3 N 4 / LSACF复合材料是降解RhB的有前途的材料。
更新日期:2019-08-30
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