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Mechanical properties and microstructure of Yb2SiO5 environmental barrier coatings under isothermal heat treatment
Journal of the European Ceramic Society ( IF 5.8 ) Pub Date : 2019-12-28 , DOI: 10.1016/j.jeurceramsoc.2019.12.057
Byung-Koog Jang , Nobuo Nagashima , Seongwon Kim , Yoon-Suk Oh , Sung-Min Lee , Hyung-Tae Kim

Yb2SiO5 (ytterbium monosilicate) top coatings and Si bond coat layer were deposited by air plasma spray method as a protection layer on SiC substrates for environmental barrier coatings (EBCs) application. The Yb2SiO5-coated specimens were subjected to isothermal heat treatment at 1400 °C on air for 0, 1, 10, and 50 h. The Yb2SiO5 phase of the top coat layer reacted with Si from the bonding layer and O2 from atmosphere formed to the Yb2Si2O7 phase upon heat treatment at 1400 °C. The oxygen penetrated into the cracks to form SiO2 phase of thermally grown oxide (TGO) in the bond coat and the interface of specimens during heat treatment. Horizontal cracks were also observed, due to a mismatch of the coefficient of thermal expansion (CTE) between the top coat and bond coat. The isothermal heat treatment improves the hardness and elastic modulus of Yb2SiO5 coatings; however, these properties in the Si bond coat were a little bit decreased.



中文翻译:

等温热处理下Yb 2 SiO 5环保阻隔涂层的力学性能和微观结构

通过空气等离子喷涂法将Yb 2 SiO 5(单硅酸y)外涂层和Si键合涂层作为保护层沉积在用于环境屏障涂层(EBC)的SiC衬底上。将涂覆有Yb 2 SiO 5的样品在1400°C的空气中进行0、1、10和50 h的等温热处理。在1400℃下进行热处理时,面涂层的Yb 2 SiO 5相与来自键合层的Si和形成气氛的O 2与形成Yb 2 Si 2 O 7相的气氛中的O 2反应。氧气渗透到裂缝中形成SiO 2热处理过程中,粘结涂层和试样界面中的热生长氧化物(TGO)的第一相。由于面涂层和粘结涂层之间的热膨胀系数(CTE)不匹配,还观察到了水平裂纹。等温热处理提高了Yb 2 SiO 5涂层的硬度和弹性模量。但是,硅键合涂层的这些性能略有下降。

更新日期:2019-12-28
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