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Synthesis and characterization of Sr-doped HAp-incorporated polyether ether ketone composite
Journal of Composite Materials ( IF 2.3 ) Pub Date : 2019-11-18 , DOI: 10.1177/0021998319888006
Anindya Pal 1 , Bhabatosh Biswas 1 , Ankita Das 2 , Arindam Chakraborty 3 , Pallab Datta 2 , Amit Roy Chowdhury 3 , Arijit Sinha 1
Affiliation  

Hydrothermally synthesized undoped and Sr-doped hydroxyapatite-dispersed polyether ether ketone composites has been fabricated by using hot isostatic pressing technique with 5, 10, 15, and 20 wt.% as the dispersoids content. The detailed structural investigation of the fabricated composites has been performed by scanning electron microscope, high-resolution transmission electron microscope, and X-ray diffraction technique that confirmed the uniform dispersion of the dispersoids with the polyether ether ketone matrix. The microindentation measurements show that the mechanical properties of the polyether ether ketone matrix improved remarkably with incorporation of the hydroxyapatite (HAp) particles. The nondestructively evaluated elastic modulus so obtained for the matrix and composites were further validated through finite element analysis. Moreover, the in vitro cytotoxic of the fabricated nanocomposites were also evaluated to assess its potential as a bioactive material.

中文翻译:

掺Sr掺HAp聚醚醚酮复合材料的合成与表征

使用热等静压技术制备了水热合成的未掺杂和 Sr 掺杂的羟基磷灰石分散聚醚醚酮复合材料,分散体含量为 5、10、15 和 20 wt.%。通过扫描电子显微镜、高分辨率透射电子显微镜和 X 射线衍射技术对制备的复合材料进行了详细的结构研究,证实了分散体与聚醚醚酮基体的均匀分散。微压痕测量表明,随着羟基磷灰石 (HAp) 颗粒的加入,聚醚醚酮基体的机械性能显着提高。通过有限元分析进一步验证了对基体和复合材料如此获得的非破坏性评估的弹性模量。
更新日期:2019-11-18
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