Synthesis of 1,2,3 triazole‐linked pyrimidines catalyzed by mg‐Al‐LDH‐immobilized‐CuI as a heterogeneous catalyst,Journal of Heterocyclic Chemistry

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Synthesis of 1,2,3 triazole‐linked pyrimidines catalyzed by mg‐Al‐LDH‐immobilized‐CuI as a heterogeneous catalyst
Journal of Heterocyclic Chemistry ( IF 2.0 ) Pub Date : 2019-12-23 , DOI: 10.1002/jhet.3772
Fatemeh Rezaeimanesh ₁ , Mohammad Bakherad ₁ , Hossein Nasr‐Isfahani ₁ , Bahram Bahramian ₁ , Soheila Naderi ₂

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A useful and efficient procedure was obtained for the synthesis of 1,2,3‐triazole‐linked pyrimidines via click reaction of propynylated pyrimidine and aromatic azides in the presence of Mg‐Al‐LDH‐immobilized‐CuI with high‐to‐excellent yields. Moreover, the prepared catalyst was characterized by the FT‐IR spectroscopy, XRD, BET, SEM, and ICP techniques. The developed synthetic technique offers numerous advantages such as a clean reaction, easy workup, high reaction yields, and short reaction time.

中文翻译：

mg-Al-LDH固定化CuI作为多相催化剂催化合成1,2,3三唑连接的嘧啶

在Mg-Al-LDH固定化CuI存在下，通过丙烯酰化的嘧啶和芳族叠氮化合物的点击反应，可以高效，高效地合成1,2,3-三唑连接的嘧啶，并具有很高的产率。。此外，通过FT-IR光谱，XRD，BET，SEM和ICP技术对制备的催化剂进行了表征。发达的合成技术具有许多优点，例如反应干净，后处理容易，反应产率高和反应时间短。

更新日期：2019-12-23

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