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Facial conversion of secondary phosphine oxides R1R2P(O)H to chlorophosphines R1R2PCl by acetyl chloride
Tetrahedron Letters ( IF 1.5 ) Pub Date : 2019-12-21 , DOI: 10.1016/j.tetlet.2019.151556 Jian-Qiu Zhang , Shangdong Yang , Li-Biao Han
中文翻译：
乙酰氯将仲膦氧化物R 1 R 2 P（O）H转化为氯膦R 1 R 2 PCl
更新日期：2019-12-21
Tetrahedron Letters ( IF 1.5 ) Pub Date : 2019-12-21 , DOI: 10.1016/j.tetlet.2019.151556 Jian-Qiu Zhang , Shangdong Yang , Li-Biao Han
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A practically useful protocol for the reductive transformation of secondary phosphine oxides R1R2P(O)H to chlorophosphines R1R2PCl using acetyl chloride was disclosed. Various secondary phosphine oxides could be readily reduced to the corresponding chlorophosphines in high yields under mild conditions. 2009 Elsevier Ltd. All rights reserved
中文翻译：
乙酰氯将仲膦氧化物R 1 R 2 P（O）H转化为氯膦R 1 R 2 PCl
公开了一种使用乙酰氯将仲膦氧化物R 1 R 2 P（O）H还原转化为氯膦R 1 R 2 PC1的实际有用的方案。在温和条件下，各种仲膦氧化物很容易以高收率还原为相应的氯膦。2009 Elsevier Ltd.保留所有权利
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