Simple reversible fixation of a magnetic catalyst in a continuous flow system: ultrafast reduction of nitroarenes and subsequent reductive amination using ammonia borane,Catalysis Science & Technology

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Simple reversible fixation of a magnetic catalyst in a continuous flow system: ultrafast reduction of nitroarenes and subsequent reductive amination using ammonia borane
Catalysis Science & Technology ( IF 4.4 ) Pub Date : 2019/12/09 , DOI: 10.1039/c9cy02021g
Hong Won Kim _{1,

2,

3,

4} , Sangmoon Byun _{4,

5,

6,

7} , Seong Min Kim _{1,

2,

3,

4} , Ha Joon Kim _{1,

2,

3,

4} , Cao Lei _{1,

2,

3,

4} , Dong Yun Kang _{1,

2,

3,

4} , Ahra Cho _{4,

5,

6,

7} , B. Moon Kim _{4,

5,

6,

7} , Jin Kyoon Park _{1,

2,

3,

4}

Affiliation

Continuous reductive amination of aldehydes with nitroarenes over a Pd–Pt–Fe₃O₄ catalyst was performed. We used NH₃BH₃ as not only a hydrogen source for nitro reduction, but also a reductant for imine reduction. Secondary aromatic amines were obtained in the continuous flow reaction in good to excellent yields.

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