The Materials Genome Initiative is expected to accelerate the materials discovery and design by fundamentally changing the trial‐and‐error research paradigm. However, mass data from high‐throughput experiments is still essential for the revelation of rules and verification of theories. In fact, the development of combinatorial materials science is always on the strength of the upgrade and evolution of high‐throughput techniques in each stage, especially high‐throughput materials synthesis and characterization. Herein, this review summarizes the high‐throughput synthesis methods for combinatorial materials libraries, especially the co‐deposition and masking techniques of thin‐film fabrication; and details the high‐throughput characterization methods for specific material properties and typical material categories, which comes down to the spectroscopy and microscopy techniques. It is considered that high‐throughput concepts will be the predominant lab experimentation in the future, along with advanced experimental techniques and convenient data processing procedures. Before that, more cooperation between multiple researchers from different fields should be conducted to complete the combinatorial materials research, since the high‐throughput technology covers multiple disciplines with a huge span.

中文翻译：

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组合材料科学中的尖端高通量合成和表征技术

材料基因组计划预计将通过从根本上改变试错研究范式来加速材料的发现和设计。然而，高通量实验的海量数据对于揭示规则和验证理论仍然至关重要。事实上，组合材料科学的发展始终依赖于各个阶段高通量技术的升级和演进，特别是高通量材料的合成和表征。在此，本文总结了组合材料库的高通量合成方法，特别是薄膜制造的共沉积和掩模技术；并详细介绍了特定材料特性和典型材料类别的高通量表征方法，这些方法归结为光谱学和显微镜技术。人们认为，高通量概念以及先进的实验技术和便捷的数据处理程序将成为未来实验室实验的主导。在此之前，由于高通量技术涉及多学科、跨度大，需要更多不同领域的研究人员进行合作来完成组合材料的研究。