Safety Considerations and Proposed Workflow for Laboratory-Scale Chemical Synthesis by Ball Milling,Organic Process Research & Development

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Safety Considerations and Proposed Workflow for Laboratory-Scale Chemical Synthesis by Ball Milling
Organic Process Research & Development ( IF 3.1 ) Pub Date : 2023-02-03 , DOI: 10.1021/acs.oprd.2c00226
Ian Priestley ₁ , Claudio Battilocchio ₂ , Andrei V. Iosub ₂ , Fabien Barreteau ₂ , Gavin W. Bluck ₂ , Kenneth B. Ling ₃ , Katharine Ingram ₃ , Maria Ciaccia ₃ , Jamie A. Leitch ₄ , Duncan L. Browne ₄

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Chemical reactions that take place in a ball mill and in the absence of a bulk reaction solvent present different safety profiles to stirred solution reactions. Herein, we present and describe steps that a researcher may take to better ensure that they have considered some of the hazards and measures that emerge and minimize the risk to themselves and their colleagues.

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