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Microstructures and mechanical properties of additively manufactured alumina ceramics with digital light processing
Archives of Civil and Mechanical Engineering ( IF 4.4 ) Pub Date : 2022-12-29 , DOI: 10.1007/s43452-022-00588-1
Mingze Xin , Zhanqiang Liu , Bing Wang , Qinghua Song

Digital light processing (DLP) technology has presented great potential to fabricate ceramic structures including alumina component, yet the mechanical properties of DLP-manufactured ceramics are still difficult to be guaranteed. The enhancement of mechanical properties of DLP-fabricated ceramic materials is challenging and imperative in the field of industrial application. This paper investigates the printing and heat treatment processes of additively manufactured ceramic to achieve defect-free Al2O3 ceramic with high performance. Firstly, Al2O3 ceramic slurry with a high solid content of 55 vol.% and viscosity of 6.04 Pa·s (at the shear rate of 100 s−1) is prepared. Then, Al2O3 ceramic is manufactured with digital light processing, debinding and sintering processes sequentially. Thirdly, the effects of sintering temperatures on the shrinkage, density, microstructure, and mechanical properties of the Al2O3 ceramics are analyzed. The shrinkage, density, and flexural strength of the sintered ceramic increase with temperature; the microhardness shows a non-monotonic trend with the increase of sintering temperature. Finally, the influence mechanism of sintering temperature on microstructures and mechanical properties of the DLP-fabricated ceramics is interpreted and discussed. The ceramic grains grow and combine to form long columnar grains during higher sintering temperatures. The density, microhardness and flexural strength of the Al2O3 ceramics sintered at 1600 °C are achieved 3.51 g/cm3, 17.71 GPa and 175.8 MPa, respectively.



中文翻译:

数字光加工增材制造氧化铝陶瓷的微观结构和力学性能

数字光处理 (DLP) 技术在制造包括氧化铝成分在内的陶瓷结构方面具有巨大潜力,但 DLP 制造的陶瓷的机械性能仍难以得到保证。提高DLP制造的陶瓷材料的机械性能在工业应用领域具有挑战性和必要性。本文研究了增材制造陶瓷的印刷和热处理工艺,以实现无缺陷的高性能Al 2 O 3陶瓷。首先,制备高固含量55vol.%、粘度6.04Pa·s(剪切速率100s -1 )的Al 2 O 3陶瓷浆料。那么,Al 2 O3陶瓷采用数字光处理、脱脂和烧结工艺依次制造。第三,分析了烧结温度对Al 2 O 3陶瓷的收缩率、密度、微观结构和力学性能的影响。烧结陶瓷的收缩率、密度和抗弯强度随温度升高而增加;随着烧结温度的升高,显微硬度呈非单调变化趋势。最后,解释和讨论了烧结温度对 DLP 制造陶瓷的微观结构和机械性能的影响机制。在较高的烧结温度下,陶瓷晶粒生长并结合形成长柱状晶粒。Al的密度、显微硬度和弯曲强度在 1600 °C 下烧结的2 O 3陶瓷分别达到 3.51 g/cm 3、17.71 GPa 和 175.8 MPa。

更新日期:2022-12-31
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