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Improved Mechanical Properties of ECAPed Mg-9Gd-2Nd-0.5Zr Alloy Through LPSO Phase Induced by Zn Addition
JOM ( IF 2.6 ) Pub Date : 2022-09-19 , DOI: 10.1007/s11837-022-05508-5
Jianzhong Gao , Xiangpeng Zhang , Hongxia Wang , Lifei Wang , Hang Li , Hua Hou , Xiaoping Luo , Kwang Seon Shin

The effect of Zn addition on the microstructure and mechanical properties of Mg-9Gd-2Nd-0.5Zr alloys during equal channel angular pressing (ECAP) was investigated. Uniformly distributed dynamically recrystallized (DRXed) grains with an average grain size of 2.7 ± 0.3 μm were obtained in the ECAPed Mg-9Gd-2Nd-0.5Zr alloy. A large number of Mg5RE phases were found to dynamically precipitate from the matrix, while the uniformly distributed dynamically recrystallized grains with an average grain size of 3.0 ± 0.3 μm were obtained in the Mg-9Gd-2Nd-1.6Zn-0.5Zr alloy. In addition, some coarse undynamically recrystallized (un-DRXed) grains existed due to the kinking of the long period stacking ordered (LPSO) phase. A small amount nano-β1 phases were dynamically precipitated from the matrix with the exception of the broken (MgZn)3RE and LPSO phase. The ECAPed Mg-9Gd-2Nd-1.6Zn-0.5Zr alloy expresses excellent comprehensive mechanical properties (YS = 321 MPa, UTS = 377 MPa, EL = 14.5%) compared with the Mg-9Gd-2Nd-0.5Zr alloy (YS = 317 MPa, UTS = 360 MPa, EL = 9.6%). This can be attributed to the strengthening and toughening effect of the LPSO phase, which not only makes the alloy exhibit a typical bimodal microstructure and improve the strength of the alloy, but also weakens the basal surface texture to improve the plasticity of the alloy.



中文翻译:

加锌诱导 LPSO 相改善 ECAPed Mg-9Gd-2Nd-0.5Zr 合金的力学性能

研究了Zn添加对Mg-9Gd-2Nd-0.5Zr合金在等通道角挤压(ECAP)过程中显微组织和力学性能的影响。在 ECAPed Mg-9Gd-2Nd-0.5Zr 合金中获得了均匀分布的动态再结晶 (DRXed) 晶粒,平均晶粒尺寸为 2.7 ± 0.3 μm。发现大量Mg 5 RE 相从基体中动态析出,而在Mg-9Gd-2Nd-1.6Zn-0.5Zr 合金中得到均匀分布的动态再结晶晶粒,平均晶粒尺寸为3.0±0.3 μm . 此外,由于长周期堆积有序(LPSO)相的扭结,存在一些粗大的非动态再结晶(非DRXed)晶粒。少量纳米β1除了破碎的 (MgZn) 3 RE 和 LPSO 相之外,其他相从基质中动态沉淀出来。ECAPed Mg-9Gd-2Nd-1.6Zn-0.5Zr 合金与 Mg-9Gd-2Nd-0.5Zr 合金 (YS = 317 兆帕,UTS = 360 兆帕,EL = 9.6%)。这可以归因于LPSO相的强韧化作用,不仅使合金呈现出典型的双峰显微组织,提高了合金的强度,而且削弱了基面织构,提高了合金的塑性。

更新日期:2022-09-20
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