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Mechanical stretching of a perfect single crystal: a routeway to a d-spacing tunable X-ray monochromator
Journal of Applied Crystallography ( IF 5.2 ) Pub Date : 2022-09-14 , DOI: 10.1107/s1600576722007452
Cesar Cusatis , Egon Piragibe Barros Silva Borges , Germán Alfredo Tirao , Marcelo Goncalves Honnicke

The feasibility of using traction forces to produce mechanical stretching/shrinkage in a perfect Si 400 single crystal is explored theoretically (by finite element analysis and dynamical theory of X-ray diffraction) and experimentally in order to use it as an angular static interplanar-distance (d-spacing) tunable monochromator, in the Bragg case. It is shown that, with traction forces of ∼100 N and an appropriate pre-load, it is possible to scan, with a linear response and reproducibility of ∼5%, a 30 eV bandwidth, which corresponds to a d-spacing scan of 7 × 10−3 Å.

中文翻译:

完美单晶的机械拉伸:通往 d 间距可调谐 X 射线单色仪的途径

在理论上(通过有限元分析和 X 射线衍射的动力学理论)和实验探索了使用牵引力在完美的 Si 400 单晶中产生机械拉伸/收缩的可行性,以便将其用作角静态晶面间距( d -spacing) 可调单色器,在布拉格的情况下。结果表明,在约 100 N 的牵引力和适当的预载荷下,可以以约 5% 的线性响应和可重复性扫描 30 eV 带宽,这对应于d间距扫描7 × 10 -3 埃。
更新日期:2022-09-14
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