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Versatile, Cheap, Readily Modifiable Sample Delivery Method for Analysis of Air-/Moisture-Sensitive Samples Using Atmospheric Pressure Solids Analysis Probe Mass Spectrometry
Analytical Chemistry ( IF 6.7 ) Pub Date : 2022-08-05 , DOI: 10.1021/acs.analchem.2c02039
Kerry A Strong 1 , Peter Stokes 1 , David Parker 1 , Amy K Buckley 1 , Jackie A Mosely 1 , Claire N Brodie 1 , Philip W Dyer 1
Affiliation  

A cheap, versatile, readily modified, and reusable glass probe system enabling delivery of solid air-/moisture-sensitive samples for mass spectrometric (MS) analysis using an Atmospheric pressure Solids Analysis Probe (ASAP) is described. The simplicity of the design allows quick and easy ASAP MS analyses of sensitive solid and liquid samples without the need for any modifications to commercially available vertically loaded ASAP mass spectrometers. A comparison of ASAP mass spectra obtained for metal complexes under air and an inert atmosphere is given.

中文翻译:

使用大气压固体分析探针质谱法分析空气/水分敏感样品的多功能、廉价、易于修改的样品输送方法

描述了一种廉价、多功能、易于修改和可重复使用的玻璃探针系统,该系统能够使用大气压固体分析探针 (ASAP) 提供对空气/水分敏感的固体样品进行质谱 (MS) 分析。设计的简单性允许对敏感的固体和液体样品进行快速简便的 ASAP MS 分析,而无需对市售的垂直加载 ASAP 质谱仪进行任何修改。给出了在空气和惰性气氛下获得的金属配合物的 ASAP 质谱比较。
更新日期:2022-08-05
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