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Synthesis of a New 1,2,4-Triazine Derived Azidoxime
Propellants, Explosives, Pyrotechnics ( IF 1.7 ) Pub Date : 2022-07-10 , DOI: 10.1002/prep.202200138 Alexander Cleveland 1 , Christopher Snyder 1 , Gregory Imler 2 , David Chavez 1 , Damon Parrish 3
Propellants, Explosives, Pyrotechnics ( IF 1.7 ) Pub Date : 2022-07-10 , DOI: 10.1002/prep.202200138 Alexander Cleveland 1 , Christopher Snyder 1 , Gregory Imler 2 , David Chavez 1 , Damon Parrish 3
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A 1,2,4-triazine based azidoxime was formed via the substitution of a chloroxime (3) with sodium azide in ethanol. This compound was characterized via single-crystal X-ray diffraction. This material has a calculated density of 1.746 g ⋅ cm−3 and is less sensitive to impact, spark, and friction, as compared to PETN and RDX. The dehydrated material has a calculated density of 1.823 g ⋅ cm−3 and the detonation pressure and velocity of 4 are calculated to be 29.1 GPa and 8.67 km ⋅ s−1, respectively.
中文翻译：
新型 1,2,4-三嗪衍生叠氮肟的合成
通过在乙醇中用叠氮化钠取代氯肟 ( 3 )形成基于 1,2,4-三嗪的叠氮肟。该化合物通过单晶 X 射线衍射进行表征。这种材料的计算密度为 1.746 g ⋅ cm -3，与 PETN 和 RDX 相比，对冲击、火花和摩擦的敏感性较低。脱水材料的计算密度为 1.823 g ⋅ cm -3，爆轰压力和速度4分别计算为 29.1 GPa 和 8.67 km ⋅ s -1。
更新日期：2022-07-10
中文翻译：
新型 1,2,4-三嗪衍生叠氮肟的合成
通过在乙醇中用叠氮化钠取代氯肟 ( 3 )形成基于 1,2,4-三嗪的叠氮肟。该化合物通过单晶 X 射线衍射进行表征。这种材料的计算密度为 1.746 g ⋅ cm -3，与 PETN 和 RDX 相比，对冲击、火花和摩擦的敏感性较低。脱水材料的计算密度为 1.823 g ⋅ cm -3，爆轰压力和速度4分别计算为 29.1 GPa 和 8.67 km ⋅ s -1。
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