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The influence of powder characteristics on densification behavior and microstructure evolution of W-Cr-Zr alloy consolidated by field-assisted sintering technology
International Journal of Refractory Metals & Hard Materials ( IF 4.2 ) Pub Date : 2022-06-25 , DOI: 10.1016/j.ijrmhm.2022.105939
W.J. Wang , X.Y. Tan , S.P. Yang , Y.R. Mao , L.M. Luo , X.Y. Zhu , A. Litnovsky , J.W. Coenen , Ch. Linsmeier , Y.C. Wu

In the present study, the influence of powder characteristics on the densification behavior and microstructure evolution of the W-Cr-Zr alloy during consolidation was investigated. The W-Cr-Zr alloy powders were prepared through mechanical alloying in different modes, i.e. continuous mechanical alloying (CMA) and intermittently mechanical alloying (IMA). It can be found that the IMA powders have a higher grain boundary density and homogenous microstructure, which exhibits a better sintering performance than the CMA powders. The IMA powders are capable of full densification and homogenization after sintering at low temperature (1395 °C), with the grain size approaching 284 nm. Through the characterization of antioxidant properties, it was confirmed that the alloy prepared using IMA powders has an excellent anti-oxidation performance.



中文翻译:

粉末特性对场辅助烧结W-Cr-Zr合金致密化行为和组织演变的影响

在本研究中,研究了粉末特性对 W-Cr-Zr 合金在固结过程中的致密化行为和显微组织演变的影响。W-Cr-Zr合金粉末通过不同方式的机械合金化制备,即连续机械合金化(CMA)和间歇机械合金化(IMA)。可以发现,IMA粉体具有更高的晶界密度和均匀的微观结构,其烧结性能优于CMA粉体。IMA粉末在低温(1395°C)下烧结后能够充分致密化和均质化,晶粒尺寸接近284 nm。通过对抗氧化性能的表征,证实使用IMA粉末制备的合金具有优异的抗氧化性能。

更新日期:2022-06-29
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