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Microstructure and mechanical properties of Ti–45Al–2W–xC alloys
Intermetallics ( IF 4.3 ) Pub Date : 2022-06-25 , DOI: 10.1016/j.intermet.2022.107618
Kateryna Kamyshnykova , Juraj Lapin , Tatiana Pelachová , Tomas Cegan , Jan Jurica , Anastasia Volodarskaja

The microstructure and mechanical properties of five alloys with nominal compositions of Ti–45Al–2W–xC (in at.%), where x is ranging from 0.4 to 2.0 at.%, were studied. The alloys were prepared by vacuum induction melting in graphite crucibles, followed by centrifugal casting into a graphite mould. The as-cast alloys were subjected to hot isostatic pressing and heat treatment consisting of solution annealing, cooling at a constant rate and stabilisation annealing. The microstructure of the heat-treated alloys consists of equiaxed α2(Ti3Al) + γ(TiAl) lamellar grains surrounded by γ grain boundaries with a small amount of β/B2 particles. The α22 interlamellar spacing λ decreases with increasing carbon content until a solubility limit of carbon is achieved. The increase in carbon content above the solubility limit leads to the formation of primary Ti2AlC particles during solidification and an increase in the amount of γ phase at grain boundaries. Vickers microhardness of lamellar grains depends on the carbon content and interlamellar spacing λ. The studied Ti–45Al–2W–0.8C and Ti–45Al–2W–1.2C alloys show improved creep resistance at 800 °C compared to that of the reference carbon-free TiAl–W and carbon-containing TiAl–Nb based alloys with fully lamellar, nearly lamellar, convoluted or pseudo-duplex microstructure.



中文翻译:

Ti-45Al-2W-xC合金的显微组织和力学性能

研究了标称成分为 Ti-45Al-2W-xC(以 at.% 为单位)的五种合金的微观结构和机械性能,其中 x 的范围为 0.4 至 2.0 at.%。这些合金是通过在石墨坩埚中真空感应熔炼制备的,然后离心铸造成石墨模具。铸态合金经过热等静压和热处理,包括固溶退火、恒速冷却和稳定退火。热处理合金的显微组织由等轴α 2 (Ti 3 Al) + γ(TiAl) 层状晶粒组成,周围有少量β/B2 颗粒的γ 晶界。α 22层间距 λ 随着碳含量的增加而减小,直到达到碳的溶解度极限。超过溶解极限的碳含量的增加导致在凝固过程中形成初级Ti 2 AlC颗粒并且在晶界处γ相的量增加。层状晶粒的维氏显微硬度取决于碳含量和层间距λ。所研究的 Ti-45Al-2W-0.8C 和 Ti-45Al-2W-1.2C 合金与参考的无碳 TiAl-W 和含碳 TiAl-Nb 基合金相比,在 800 °C 下表现出更高的抗蠕变性完全层状、近层状、卷曲或假双相微结构。

更新日期:2022-06-26
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