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A Study on Electrical Properties of Nanofiber Composites: Effects of PCL/AgNO3/ZnO Concentration Percentages
Iranian Journal of Science and Technology, Transactions A: Science ( IF 1.4 ) Pub Date : 2022-05-31 , DOI: 10.1007/s40995-022-01299-1
Unal Kurt , Selcuk Atis , Zuhal Polat , Mehmet Tektas , Umit K. Terzi

Nanofibers with multifunctional properties hold great promise as they allow components for a wide range of medical applications. In this study, zinc oxide, silver nitrate and Polycaprolactone were used in the production of nanofiber composite material by coaxial electrospinning process. PCL concentrations of 5, 10, and 15% by weight were utilized in all of the samples, and different amounts of silver nitrate and zinc oxide were used. Functional groups of silver nitrate, zinc oxide, and Polycaprolactone materials were determined by Fourier transform infrared spectroscopy. Morphological analyzes were carried out with scanning electron microscopy. For all solutions, before coaxial electrospinning, physical properties such as density, liquid state ac conductivity, and viscosity were measured. For the 20 Hz–3 MHz frequency range, after coaxial electrospinning, D-factors and capacitance of nanofiber composite materials were measured and dielectric loss, permittivity, and the solid-state alternating current conductivity were calculated for all solutions. The effects of silver nitrate, zinc oxide, and Polycaprolactone concentration percentages on the solid-state ac conductivity and the dielectric constant were analyzed and comparisons were made with the results obtained.



中文翻译:

纳米纤维复合材料的电性能研究:PCL/AgNO3/ZnO 浓度百分比的影响

具有多功能特性的纳米纤维具有很大的前景,因为它们允许组件用于广泛的医疗应用。本研究以氧化锌、硝酸银和聚己内酯为原料,采用同轴静电纺丝工艺制备纳米纤维复合材料。在所有样品中使用 5、10 和 15% 重量的 PCL 浓度,并使用不同量的硝酸银和氧化锌。通过傅里叶变换红外光谱测定硝酸银、氧化锌和聚己内酯材料的官能团。用扫描电子显微镜进行形态学分析。对于所有溶液,在同轴静电纺丝之前,测量了密度、液态交流电导率和粘度等物理特性。对于 20 Hz–3 MHz 频率范围,在同轴静电纺丝后,测量了纳米纤维复合材料的 D 因子和电容,并计算了所有溶液的介电损耗、介电常数和固态交流电导率。分析了硝酸银、氧化锌和聚己内酯的浓度百分比对固态交流电导率和介电常数的影响,并与所得结果进行了比较。

更新日期:2022-05-31
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