A highly dispersed Ni₃P/HZSM-5 catalyst was prepared by deposition-precipitation of Ni species followed by electroless plating and thermal treatment, and characterized by means of XRD, ICP, N₂ physical adsorption, TEM, XPS, NH₃-TPD, and CO chemisorption. Electroless plating reaction takes place in an aqueous solution under mild conditions, facilitating the high dispersion of the formed Ni₃P particles. XRD measurements illustrated the lamellar nickel phyllosilicate was produced at the first step of deposition-precipitation, amorphous Ni-P was formed in the subsequent electroless plating, and highly dispersed Ni₃P crystallites were generated in thermal treatment. TEM observation demonstrated that the average particle size of Ni₃P crystallites in the prepared Ni₃P/HZSM-5 catalyst was 4.3 nm. Bifunctional Ni₃P/HZSM-5 was investigated in hydrodeoxygenation (HDO) of phenolic compounds, including phenol, m-cresol, and guaiacol. Ni₃P/HZSM-5 exhibited high catalytic performance in HDO with enhanced hydrogenation and dehydration pathway.

采用沉积-沉淀Ni物质、化学镀和热处理制备高分散Ni ₃ P/HZSM-5催化剂，并通过XRD、ICP、N ₂物理吸附、TEM、XPS、NH ₃ -TPD等手段对其进行表征。 , 和 CO 化学吸附。化学镀反应发生在温和条件下的水溶液中，有利于形成的Ni ₃ P颗粒的高度分散。XRD 测量表明，在沉积-沉淀的第一步产生了层状的页硅酸镍，在随后的化学镀中形成了非晶态 Ni-P，并且高度分散的 Ni ₃P微晶在热处理中产生。_{TEM观察表明，制备的Ni 3} P/HZSM-5催化剂中Ni ₃ P微晶的平均粒径为4.3 nm。在酚类化合物（包括苯酚、间甲酚和愈创木酚）的加氢脱氧 (HDO) 中研究了双功能 Ni _{3 P/HZSM-5。}Ni ₃ P/HZSM-5 在 HDO 中表现出高催化性能，具有增强的加氢和脱水途径。