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Thermophysical and structural properties of manganese ferrite nanoparticles
Modern Physics Letters B ( IF 1.8 ) Pub Date : 2021-11-29 , DOI: 10.1142/s0217984921505424 A. F. Gochuyeva 1, 2
Modern Physics Letters B ( IF 1.8 ) Pub Date : 2021-11-29 , DOI: 10.1142/s0217984921505424 A. F. Gochuyeva 1, 2
Affiliation
This paper discusses the results of the research carried out to study the structure, optical properties and thermophysical properties of a sample (nanopowder with a true density of 4.96 g/cm3, a particle size of 60 nm and a purity of 98.5%, SkySpring Nanomaterials, USA) with high purity. Based on the results of X-ray diffraction, the crystalline phase of MnFe2O4 ferrite nanoparticles was completely obtained and the values of the lattice parameters were determined. The results of the MID-IR analysis showed that the absorption coefficient ( α ) reaches its maximum value at 748 cm− 1 wave number. The optical properties of the as-prepared nanostructures were also investigated by VERTEX 70 V diffuse reflectance spectroscopy (DRS). As can be seen from the results of the DSC analysis, the effects occurring in the temperature range up to 3 0 0 ∘ C clearly reflect the nature of the phase transitions and the amount of energy generated in the ferrite samples.
中文翻译:
锰铁氧体纳米粒子的热物理和结构特性
本文讨论了为研究样品(真密度为 4.96 g/cm 3,粒径为 60 nm,纯度为 98.5% 的纳米粉末,SkySpring纳米材料,美国)具有高纯度。根据X射线衍射结果,完全得到了MnFe 2 O 4铁氧体纳米粒子的晶相,并确定了晶格参数值。中红外分析结果表明,吸收系数( α ) 在 748 厘米处达到最大值- 1 波数。还通过 VERTEX 70 V 漫反射光谱 (DRS) 研究了所制备的纳米结构的光学性质。从 DSC 分析的结果可以看出,在高达3 0 0 ∘ C 清楚地反映了相变的性质和铁氧体样品中产生的能量。
更新日期:2021-11-29
中文翻译:
锰铁氧体纳米粒子的热物理和结构特性
本文讨论了为研究样品(真密度为 4.96 g/cm 3,粒径为 60 nm,纯度为 98.5% 的纳米粉末,SkySpring纳米材料,美国)具有高纯度。根据X射线衍射结果,完全得到了MnFe 2 O 4铁氧体纳米粒子的晶相,并确定了晶格参数值。中红外分析结果表明,吸收系数