Milk and dairy products are considered as essential sources of lipid-soluble vitamins (LSVs) for human nutrition. Due to the lower concentrations, complexity, and instability of LSVs during extraction, their quantification remains challenging. This review focus on advances in the extraction and quantification of LSVs from different dairy products. Saponification, and liquid-liquid (LLE), solid-phase (SPE), and supercritical fluid (SFE) extraction methods, as well as dispersive liquid-liquid microextraction, are the most common techniques. Liquid chromatography-mass spectrophotometry (LC-MS) has unique advantages for LSVs determination and quantification due to its high sensitivity and specificity.

牛奶和乳制品被认为是人体营养所需的脂溶性维生素 (LSV) 的重要来源。由于 LSV 在提取过程中的浓度较低、复杂性和不稳定性，它们的量化仍然具有挑战性。本综述重点关注从不同乳制品中提取和量化 LSV 的进展。皂化、液-液 (LLE)、固相 (SPE) 和超临界流体 (SFE) 萃取方法以及分散液-液微萃取是最常用的技术。液相色谱-质谱法 (LC-MS) 由于其高灵敏度和特异性，在 LSV 的测定和定量方面具有独特的优势。