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Optimization and modeling of rheological characteristics for graphene-gear oil based nanolubricant using response surface methodology
Colloids and Surfaces A: Physicochemical and Engineering Aspects ( IF 4.9 ) Pub Date : 2021-09-23 , DOI: 10.1016/j.colsurfa.2021.127605
Gaurab Kumar Ghosh 1 , Ankit Kotia 2 , Niranjan Kumar 3 , Subrata Kumar Ghosh 1
Affiliation  

This article presents the experimental evaluation of rheological characteristics of graphene-gear oil (SAE EP-90) nanolubricant under varying concentration, temperature and shear rates.The nanolubricant samples have been prepared at concentrations varying from 0.3% to 1.8%. Aging test confirms good stability of the prepared nanolubricant samples even after an interval of 50 days. The rheological properties of the samples have been investigated over a temperature range of 25–80 °C and shear rate of 10–200 (1/s). Central Composite Design (CCD) of response surface methodology (RSM) was used for the experimental framework. A combination of concentration, temperature, shear rate (1.00594%, 25.0053 °C, 88.0967 (1/s)) yielded the maximum value of viscosity i.e. 396.113 mPa.s whereas the set (0.58333%, 65.5 °C, 118 (1/s)) gave the minimum value of viscosity i.e. 15.87 mPa s using Response Surface Methodology (RSM). A mathematical correlation with R2 (0.9919) has been proposed to predict the relative viscosity of the nanolubricant using analysis of variance (ANOVA) which resembles closely with the experimental data (least deviation 0.256%).



中文翻译:

基于响应面法的石墨烯-齿轮油基纳米润滑剂流变特性优化与建模

本文介绍了石墨烯齿轮油 (SAE EP-90) 纳米润滑剂在不同浓度、温度和剪切速率下的流变特性的实验评估。纳米润滑剂样品的制备浓度为 0.3% 至 1.8%。老化测试证实,即使间隔 50 天,所制备的纳米润滑剂样品仍具有良好的稳定性。已在 25–80 °C 的温度范围和 10–200 (1/s) 的剪切速率下研究了样品的流变特性。响应面方法 (RSM) 的中心复合设计 (CCD) 用于实验框架。浓度、温度、剪切速率 (1.00594%, 25.0053 °C, 88.0967 (1/s)) 的组合产生了粘度的最大值,即 396.113 mPa.s 而设置 (0.58333%, 65.5 °C, 118 (1/s)) 给出了使用响应面方法 (RSM) 的最低粘度值,即 15.87 mPa s。与 R 的数学相关性2 (0.9919) 已被提议使用方差分析 (ANOVA) 来预测纳米润滑剂的相对粘度,该分析与实验数据非常相似(最小偏差 0.256%)。

更新日期:2021-09-29
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