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Excellent gas-sensitive properties towards acetone of In2O3 nanowires prepared by electrospinning
Colloid and Interface Science Communications ( IF 4.7 ) Pub Date : 2021-09-15 , DOI: 10.1016/j.colcom.2021.100508
Yanhan Che 1 , Guoqing Feng 1 , Tianjun Sun 2 , Jingkun Xiao 1 , Weijun Guo 1 , Chengwen Song 1
Affiliation  

In2O3 nanowires (NWs) were successfully synthesized by electrospinning. The crystalline phase, microstructure, morphology, elemental composition, and BET surface area were analyzed XRD, SEM, TEM, XPS, and nitrogen adsorption. The characterization of the In2O3 NWs showed that In2O3 NWs were uniform thickness, structural integrity, and high purity. In subsequent gas-sensitive tests, the effects of PVP percentage, calcination temperature, calcination ramp-up rate, and calcination time on sensitive properties were analyzed. In particular, the In2O3 sensor showed a response of up to 37.9 (Ra/Rg) to 100 ppm acetone at an operating temperature of 200 °C and the response/recovery time is 1 s/7 s. The gas-sensitive mechanism of the In2O3 sensor was also analyzed in conjunction with the characterization results. Our study shows that the response of the In2O3 sensor is improved compared to the previously published sensors.



中文翻译:

静电纺丝制备的 In2O3 纳米线对丙酮具有优异的气敏性能

通过静电纺丝成功合成了In 2 O 3纳米线(NW)。通过XRD、SEM、TEM、XPS和氮吸附分析了晶相、微观结构、形貌、元素组成和BET表面积。In 2 O 3纳米线的表征表明,In 2 O 3纳米线具有均匀的厚度、结构完整性和高纯度。在随后的气敏试验中,分析了 PVP 百分比、煅烧温度、煅烧升温速率和煅烧时间对敏感性能的影响。特别是,In 2 O 3在 200 °C 的工作温度下,传感器对 100 ppm 丙酮的响应高达 37.9 (Ra/Rg),响应/恢复时间为 1 秒/7 秒。还结合表征结果分析了 In 2 O 3传感器的气敏机制。我们的研究表明,与之前发布的传感器相比,In 2 O 3传感器的响应得到了改进。

更新日期:2021-09-15
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