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Enhancing permeability and porosity of ceramic shells for investment casting through pre-wetting
Journal of the European Ceramic Society ( IF 5.7 ) Pub Date : 2021-09-10 , DOI: 10.1016/j.jeurceramsoc.2021.09.022
Noel O’Sullivan 1 , Joseph Mooney 1 , David Tanner 1
Affiliation  

In this study, a method known as pre-wetting is applied between the multilayer ceramic investment casting shells to enhance porosity and permeability while sustaining flexural strength. Pre-wetting consists predominately of an aqueous silica binder that improves inter-coat bonding in complex areas. Porosity is developed where the pre-wetting is applied due to the evaporation of the aqueous phase. Results indicate that as porosity increases, both green and fired flexural strength reduce on average by 8.7 - 15.6 % and 18.7 - 28.5 %, respectively, whereas hot strength is increased by 20 - 25 %. Permeability increased by a factor of two when pre-wetting was applied between intermediate coatings and displayed a stepwise increase in intrusion volume in the high-pressure regime through mercury intrusion porosimetry. X-ray microtomography coupled with pore network modelling provided a validation of the increase in the permeability constant. Gas adsorption methods revealed the presence of micropores through the alpha-s method when bilayers of pre-wetting solution were applied.



中文翻译:

通过预湿提高熔模铸造用陶瓷壳的渗透性和孔隙率

在这项研究中,一种称为预润湿的方法应用于多层陶瓷熔模铸造壳之间,以提高孔隙率和渗透率,同时保持抗弯强度。预润湿主要由水性二氧化硅粘合剂组成,可改善复杂区域的涂层间粘合。由于水相的蒸发,在进行预润湿的地方会产生孔隙。结果表明,随着孔隙率的增加,生坯和烧制弯曲强度平均降低 8.7—— 15.6% 和 18.7 —— 分别为 28.5 %,而热强度提高了 20 ——25%。当在中间涂层之间应用预润湿时,渗透率增加了两倍,并且通过压汞孔隙率测定法在高压状态下显示出侵入量的逐步增加。X 射线显微断层扫描与孔隙网络建模相结合,验证了渗透率常数的增加。当应用预润湿溶液的双层时,气体吸附方法通过 alpha-s 方法揭示了微孔的存在。

更新日期:2021-10-19
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