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Synthesis of 6,7-dihydro-4H-[1,2,3]triazolo[5,1-c][1,4]oxazines via tandem reactions of β-iodoazides with propargyl alcohols
Synthetic Communications ( IF 1.8 ) Pub Date : 2021-08-25 , DOI: 10.1080/00397911.2021.1968905
Xiao-Lan Zhang 1 , Guo-Qiao Qiu 2 , Jun-Min Chen 3 , Shou-Ri Sheng 3
Affiliation  

Abstract

Tandem reactions between β-iodoazides and propargyl alcohols under mild conditions are presented, providing a general and convenient method for the synthesis of 6,7-dihydro-4H-[1,2,3]triazolo[5,1-c][1,4]oxazines. The advantages of this method are its simple operation, high efficiency and high product yields (80–95%).



中文翻译:

通过β-碘叠氮化物与炔丙醇的串联反应合成6,7-二氢-4H-[1,2,3]三唑并[5,1-c][1,4]恶嗪

摘要

介绍了β-碘叠氮化物和炔丙醇在温和条件下的串联反应,为合成6,7-二氢-4 H- [1,2,3]三唑并[5,1- c ][提供了一种通用方便的方法。1,4]恶嗪。该方法的优点是操作简单、效率高、产品收率高(80-95%)。

更新日期:2021-11-03
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