当前位置: X-MOL 学术J. Sol-Gel Sci. Technol. › 论文详情
Our official English website, www.x-mol.net, welcomes your feedback! (Note: you will need to create a separate account there.)
Preparation and characterization of (Zr0.8,Sn0.2)TiO4 nano crystals by hydrothermal-molten salt method
Journal of Sol-Gel Science and Technology ( IF 2.5 ) Pub Date : 2021-07-08 , DOI: 10.1007/s10971-021-05581-3
Qi Wu 1 , Xiangchun Liu 1 , Zhengguang Li 1 , Li Qiang 1 , Ningna Bai 1 , Kai Zhang 1 , Zhe Yang 1
Affiliation  

The pure phase (Zr0.8,Sn0.2)TiO4 nano crystals have been prepared by hydrothermal-molten salt method. The effects of the pH of solvent system, the calcinations temperature and the ratio of composite molten salt on the phase composition and crystalline morphology have been investigated. The results show that the high pure phase (Zr0.8,Sn0.2)TiO4 nano crystals with regular morphology were prepared at 1000 oC in NaCl-KCl salt system. The synthesized temperature of single phase (Zr0.8,Sn0.2)TiO4 is lower and the crystal growth is more complete compared with the hydrothermal-solid state method. The rod-like crystalline grain are evenly distributed with a diameter of about 50–60 nm and can be used as start materials for preparing ZST textured ceramics. The (Zr0.8,Sn0.2)TiO4 nano crystal has a certain photocatalytic effect and good UV shielding performance.



中文翻译:

水热-熔盐法制备(Zr0.8,Sn0.2)TiO4纳米晶体及其表征

采用水热熔盐法制备了纯相(Zr 0.8 ,Sn 0.2 )TiO 4纳米晶体。研究了溶剂体系的pH值、煅烧温度和复合熔盐比例对相组成和结晶形貌的影响。结果表明,高纯相(锆0.8,锡0.2)的TiO 4纳米晶体具有规则的形态在1000制备 Ô在NaCl-KCl的盐系C。单相(Zr 0.8 ,Sn 0.2 )TiO 4的合成温度与水热固相法相比,晶体生长更完全。棒状晶粒分布均匀,直径约50-60 nm,可作为制备ZST织构陶瓷的起始材料。(Zr 0.8 ,Sn 0.2 )TiO 4纳米晶体具有一定的光催化作用和良好的紫外线屏蔽性能。

更新日期:2021-07-08
down
wechat
bug