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[DMImd-DMP]: A highly efficient and reusable catalyst for the synthesis of 4H-benzo[b]pyran derivatives
Heterocyclic Communications ( IF 1.3 ) Pub Date : 2019-12-31 , DOI: 10.1515/hc-2019-0025
Mohamed Abdenour Redouane 1 , Naima Khiri-Meribout 1 , Saida Benzerka 1 , Abdelmadjid Debache 1
Affiliation  

Abstract A series of substituted 4H-pyrans derivatives were synthesized by a one-pot, multi-component reaction of aromatic aldehydes, malononitrile, and pyrazolone derivatives or active methylene carbonyl compounds such as dimedone, in the presence of 1,3-dimethyl imidazolium dimethyl phosphate [DMImd-DMP] as a catalyst in aqueous ethanol. Recyclability of the catalyst, high yields, simple product isolation and high atom economy are the noteworthy aspects of this protocol.

中文翻译:

[DMIMd-DMP]:一种高效且可重复使用的催化剂,用于合成 4H-苯并[b]吡喃衍生物

摘要 以芳香醛、丙二腈和吡唑啉酮衍生物或活性亚甲基羰基化合物如二甲酮为原料,在1,3-二甲基咪唑鎓二甲基吡啶存在下,通过一锅多组分反应合成了一系列取代的4H-吡喃衍生物。磷酸盐 [DMImd-DM​​P] 作为乙醇水溶液中的催化剂。催化剂的可回收性、高产率、简单的产品分离和高原子经济性是该协议值得注意的方面。
更新日期:2019-12-31
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