Abstract

A novel organic α,β unsaturated carbonyl compound (Z)-2-((3-(4-chlorophenyl)-1-phenyl-1H-pyrazol-4-yl)methylene)-3,4-dihydronaphthalen-1(2H)-one (K) was Synthesized through Ultrasound Irradiation by the help of green solvent and grown a high quality single crystal by slow evaporation method. Structural confirmation was carried out by most acceptable spectroscopic techniques i.e. MS, IR, NMR, CMR, DSC, Crystal Structure of K was determined by single crystal X-ray Diffraction. The single crystal of K was developed in 0.40 × 0.35 × 0.30 mm dimension in EtOH:Acetone (1:2) solvent system. K crystallizes in the monoclinic crystal class in the asymmetrical space group with Z = 4. Potency of compound was assayed against four bacterial microorganisms.

摘要

一种新型有机α,β不饱和羰基化合物（Z）-2-（（3-（4-氯苯基）-1-苯基-1H-吡唑-4-基）亚甲基）-3,4-二氢萘-1（2H） -one (K) 是在绿色溶剂的帮助下通过超声辐照合成的，并通过缓慢蒸发的方法生长出高质量的单晶。结构确认通过最可接受的光谱技术进行，即 MS、IR、NMR、CMR、DSC，K 的晶体结构通过单晶 X 射线衍射确定。K 的单晶在 EtOH:丙酮 (1:2) 溶剂系统中以 0.40 × 0.35 × 0.30 mm 尺寸开发。K 在Z  = 4的不对称空间群中的单斜晶体类中结晶。针对四种细菌微生物测定了化合物的效力。