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Role of virgin coconut oil (VCO) as co-extractant for obtaining xanthones from mangosteen (Garcinia mangostana) pericarp with supercritical carbon dioxide extraction
The Journal of Supercritical Fluids ( IF 3.4 ) Pub Date : 2021-05-20 , DOI: 10.1016/j.supflu.2021.105305
Siew Lee Kok , Wan Jun Lee , Richard Lee Smith , Norhidayah Suleiman , Kriskamol Na Jom , Kanithaporn Vangnai , Amir Hamzah Bin Sharaai , Gun Hean Chong

Virgin coconut oil (VCO) was used as co-extractant with supercritical carbon dioxide (scCO2) extraction for obtaining xanthones from mangosteen pericarp (MP) without organic co-solvents. In each experiment, 120 g of dried MP that had median particle sizes of 0.85 mm was used. Extraction of MP with 40% VCO co-extractant using scCO2 (1.08 kg/h) for 420 min at 430 bar and 70 °C gave α-mangostin (32.2 mg/g), γ-mangostin (7.2 mg/g), xanthones (28.2 mg/g) in extract and an extraction yield of 31%. The role of VCO is that it promotes dissolution of xanthones and mass transfer into the scCO2 phase as elucidated with the Pardo-Castaño model. The Lentz equation was generalized in terms of (P, T, %VCO, ρCO2) to correlate all extraction curve data to within 7.4% and to estimate extraction yield crossover regions. Xanthones can be separated from mangosteen pericarp with VCO and scCO2 extraction without organic co-solvents.



中文翻译:

初榨椰子油(VCO)作为共提取物通过超临界二氧化碳萃取从山竹果皮(Garcinia mangostana)果皮中获得氧杂蒽酮的作用

初榨椰子油(VCO)与超临界二氧化碳(scCO 2)一起用作共萃取剂,用于从山竹果皮(MP)中获得没有有机助溶剂的黄酮。在每个实验中,使用具有中值粒度为0.85mm的120g干燥的MP。在430 bar和70°C下使用scCO 2(1.08 kg / h)于420分钟内用40%VCO共萃取剂提取MP,得到α-芒果素(32.2 mg / g),γ-芒果素(7.2 mg / g),提取物中的氧杂蒽酮(28.2 mg / g)和提取产率为31%。如Pardo-Castaño模型所阐明的,VCO的作用是促进氧杂蒽的溶解和质子转移到scCO 2相中。Lentz方程用(PŤ,%VCO,ρ CO2)相关联的所有的提取曲线数据至7.4%的范围内,并估计提取率交叉区域。可以在不使用有机助溶剂的情况下,通过VCO和scCO 2萃取从山竹果皮中分离出Xanthones 。

更新日期:2021-05-27
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