Self-organized TiOF₂ nanotubes have been synthesized by a one-pot solvothermal method. Different solvent ratios have been used during material preparation. When choosing the equal ratios of acetic acid and trifluoroacetic acid (TFA) as the solvent, uniform TiOF₂ nanotubes were obtained. It is found that the solvent ratios alter their crystalline nature and surface morphology. X-ray diffraction (XRD) pattern indicates that the sample is pure and single-crystalline in nature. Scanning electron microscopy (SEM) morphology points out that the TiOF₂ nanotubes with a length of approximately 2–3 μm, which composed of self-assembled nanorods. This distinct construction is advantageous to enhance the photocatalytic hydrogen (H₂) evolution under UV–vis irradiation. Photocatalytic examination reveals that the TiOF₂ nanotubes have a high photocatalytic H₂ evolution rate (~800 μmol h⁻¹ g⁻¹) than other attempted candidates. The excellent photocatalytic H₂ evolution attributes to the tube-like morphology and large separations of charge carriers.

通过一锅溶剂热法合成了自组织的TiOF ₂纳米管。在材料制备过程中已使用了不同的溶剂比例。When choosing the equal ratios of acetic acid and trifluoroacetic acid (TFA) as the solvent, uniform TiOF ₂ nanotubes were obtained. 发现溶剂比例改变了它们的结晶性质和表面形态。X射线衍射（XRD）图表明样品是纯净的单晶。扫描电子显微镜（SEM）形态指出，TiOF ₂纳米管的长度约为2-3μm，由自组装的纳米棒组成。这种独特的结构有利于增强光催化氢（H ₂）在紫外线可见辐射下的演变。光催化检查显示，TiOF ₂纳米管比其他尝试的候选物具有更高的光催化H ₂释放速率（〜800μmolh ^-1  g ^-1）。优异的光催化H ₂析出归因于管状形态和载流子的大分离。