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Growth and XRD, Elemental, Mechanical, Dielectric, Optical and Photoconductivity, and Surface Morphological Characterizations of 2-[4-(Trifluoromethyl) phenyl]-1H-benzimidazole (TFMPHB) Crystals for Electronic, Mechanical Applications
Brazilian Journal of Physics ( IF 1.5 ) Pub Date : 2021-03-29 , DOI: 10.1007/s13538-021-00883-x
R. P. Patel , K. SenthilKannan , R. Hariharasuthan , S. Gunasekaran , R. Divya , P. Periasamy , N. Y. Maharani

Nonlinear optical crystalline material is the fascinating tool for the optoelectronic devices and for phase-matched equipments, frequency matching circuits and etc. Present study portrays the synthesize and utility of macro and nano scaled crystals of 2-[4-(trifluoromethyl) phenyl]-1H-benzimidazole (TFMPHB) by slow evaporation solution growth method and by milling conversion. As-prepared crystals were studied by XRD, CHNSO analysis, dielectric and tribology-mechanical, NLO, and photoconductivity. The orthorhombic phase structure with the average crystalline size of 21 nm was observed. The elemental composition of crystals was analyzed for the presence of elements. Tribological studies of macro and nano TFMPHB crystals were favorable for mechanical applications. Further, the high dielectric constant (363 K) at low frequency was suitable for microelectronic devices; NLO is analyzed with phase matching effect over particle size, and photoconductivity study also reported for the entitled crystalline specimen. The structural parameters by AFM and SEM, absorbance nature by UV spectra, and modeling data by computational methods are also reported.



中文翻译:

2- [4-(三氟甲基)苯基] -1H-苯并咪唑(TFMPHB)晶体的生长和XRD,元素,机械,介电,光电导和光电导以及表面形态学表征,用于电子,机械应用

非线性光学晶体材料是光电器件,相位匹配设备,频率匹配电路等的引人入胜的工具。本研究描述了2- [4-(三氟甲基)苯基]-的大尺寸和纳米级晶体的合成和实用性。 1H-苯并咪唑(TFMPHB)通过缓慢蒸发溶液生长方法和通过研磨转化而得。通过XRD,CHNSO分析,介电和摩擦学-机械学,NLO和光电导性研究了制备的晶体。观察到正交晶体相结构,其平均晶体大小为21 nm。分析晶体的元素组成中是否存在元素。宏观和纳米TFMPHB晶体的摩擦学研究对于机械应用是有利的。更多,低频时的高介电常数(363 K)适用于微电子设备;对NLO进行了粒度相匹配的分析,并报道了标题晶体样品的光电导性研究。还报道了通过AFM和SEM的结构参数,通过UV光谱的吸收性质以及通过计算方法的建模数据。

更新日期:2021-04-23
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