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Study of Ag2O/TiO2 nanowires synthesis and characterization for heterogeneous reduction reaction catalysis of 4-nitrophenol
Nano-Structures & Nano-Objects Pub Date : 2021-04-01 , DOI: 10.1016/j.nanoso.2021.100719
Rika Tri Yunarti , Ilham Deryansyah Isa , Lizbeth Cantik Christina Dimonti , Adid Adep Dwiatmoko , Muhammad Ridwan , Jeong-Myeong Ha

Ag2O/TiO2 nanowires as catalyst for reduction reaction of 4-nitrophenol has been synthesized in this study with molten-salt route and followed by the impregnation method. Analysis by characterization results show that the addition of Ag2O does not change TiO2 crystal structure and morphology, and it was found that the impregnated Ag2O has metal-support interactions with TiO2 nanowires. Size distribution of TiO2 nanowires structure along with the Ag2O is known to be within the range of nanomaterial. TiO2 nanowires has an average width of 339.706 nm, and the impregnated Ag2O has an average diameter size of 19.873 nm respectively. The catalytic test performance shows that Ag2O/TiO2 nanowires has excellent result compared to the control sample morphology of Ag2O/TiO2 anatase. It is closely correlated with the electron transfer capability of TiO2 nanowires structure and this shows that Ag2O/TiO2 nanowires is suitable for catalysis of 4-nitrophenol reduction reaction.



中文翻译:

Ag 2 O / TiO 2纳米线的合成及表征4-硝基苯酚的非均相还原反应研究

本研究采用熔融盐法合成了Ag 2 O / TiO 2纳米线作为4-硝基苯酚还原反应的催化剂,并采用了浸渍法。通过表征结果分析表明,Ag 2 O的添加不会改变TiO 2的晶体结构和形态,并且发现浸渍的Ag 2 O与TiO 2纳米线具有金属-载体相互作用。已知TiO 2纳米线结构与Ag 2 O一起的尺寸分布在纳米材料的范围内。TiO 2纳米线的平均宽度为339.706 nm,浸渍的Ag 2O的平均直径尺寸分别为19.873nm。催化测试性能表明,与控制样品形态的Ag 2 O / TiO 2锐钛矿相比,Ag 2 O / TiO 2纳米线具有优异的结果。它与TiO 2纳米线结构的电子传递能力密切相关,这表明Ag 2 O / TiO 2纳米线适用于催化4-硝基苯酚还原反应。

更新日期:2021-04-01
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