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Properties analysis of crosslinked chitosan microcapsules by multiple emulsification method
Fashion and Textiles ( IF 2.3 ) Pub Date : 2021-02-25 , DOI: 10.1186/s40691-020-00230-9
Su-Jin Ryu , Hyun-Sook Bae

Chemical based finishing agents often affect human body and environment. Therefore, in this study, eco-friendly microcapsules were manufactured to minimize the use of chemicals by using chitosan, a natural substance, as a wall material and basil oil as a core material. First, the optimum manufacturing conditions were established through the shape and size of the synthesized microcapsules. Second, the synthesis and thermal stability of the prepared microcapsules were evaluated. Finally, the applicability to functional fiber processing was reviewed by measuring the release characteristics of the microcapsules. Consequently, using 2 wt% chitosan, Triton X-100 as a emulsifier and stirring at 6000 rpm were considered to be efficient in terms of capsule formation. FT-IR spectrum and Gas Chromatograph showed that microcapsules were stably synthesized. And microcapsule containing basil oil was given heat resistance by encapsulation. Lastly, microcapsules can be confirmed to have sustained-release, due to basil oil in microcapsules has a small amount of release up to 10 h, and is continuously released until after 60 h to release slowly, As a result, the manufactured microcapsules finishing agent may be applied to finishing of textile product.

中文翻译:

多重乳化法研究交联壳聚糖微胶囊的性能

化学基整理剂通常会影响人体和环境。因此,在这项研究中,通过使用天然物质壳聚糖作为墙体材料和罗勒油作为核心材料,制造了环保型微胶囊,以最大程度地减少化学药品的使用。首先,通过合成微胶囊的形状和大小确定了最佳制造条件。其次,评估了所制备的微胶囊的合成和热稳定性。最后,通过测量微胶囊的释放特性,回顾了其对功能性纤维加工的适用性。因此,就胶囊形成而言,认为使用2重量%的壳聚糖,Triton X-100作为乳化剂并以6000rpm搅拌是有效的。傅立叶变换红外光谱和气相色谱仪表明,微囊是稳定合成的。并且,通过包封使含有罗勒油的微胶囊具有耐热性。最后,由于微胶囊中的罗勒油在10小时内有少量释放,因此可以确认微胶囊具有持续释放,并持续释放直至60小时后才缓慢释放,因此,制得的微胶囊整理剂可用于纺织品的后整理。
更新日期:2021-02-26
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