The prepared Fe₃O₄/multiwalled carbon nanotubes (MWCNTs) in catalytic wet peroxide oxidation (CWPO) is an effective method of removing some pharmaceuticals from water matrices for environmental protection. Therefore, operating parameters (catalyst dose, H₂O₂ dose, flow rate, pH) of CWPO with the easy-prepared Fe₃O₄/MWCNT composite were evaluated for the effective NAP removal in an up-flow bed reactor (UFBR). The prepared catalyst was successfully synthesized by a facile coprecipitation method. The highest removals of TOC and NAP by continuous CWPO of NAP aqueous solution (10 mg L⁻¹) were obtained in the experiments with ratios 0.4 g of catalyst load/double H₂O₂ stoichiometric ratio (78.4% for TOC and 83% for NAP), and 0.2 g of catalyst load/stoichiometric dose (39.1% for TOC and 73.1% for NAP). Both operated at 10 mg L⁻¹ of NAP, 1.7 mL min⁻¹, 50 °C and circumneutral pH. In addition, their high consumption H₂O₂ efficiency (> 59.6%) and a low concentration of leached iron dissolved (< 0.28 mg L⁻¹) found at 450 min indicated the great catalyst stability. Furthermore, the application of CWPO for different aqueous matrices, the NAP removal from in a surface water sample was almost complete (90.5%) 1260 min TOS while whereas in the hospital wastewater and wastewater treatment plant effluent samples were 64.9% and 58.9%, respectively. Our results demonstrate that continuous CWPO with the easy-prepared Fe₃O₄/MWCNTs has the potential to be applied as an effective treatment for the rapid removal of NAP from different water matrices.

催化湿式过氧化物氧化（CWPO）制得的Fe ₃ O ₄ /多壁碳纳米管（MWCNTs）是从水基质中去除某些药物的一种有效方法，以保护环境。因此，对易于制备的Fe ₃ O ₄ / MWCNT复合材料的CWPO的运行参数（催化剂剂量，H ₂ O ₂剂量，流速，pH）进行了评估，以评估其在上流床反应器（UFBR）中的有效NAP去除率。 。所制备的催化剂通过简便的共沉淀法成功合成。NAP水溶液的连续CWPO对TOC和NAP的去除最高（10 mg L ^-1在实验中以0.4 g的催化剂负载/双H ₂ O ₂化学计量比（TOC为78.4％，NAP为83％）和0.2 g的催化剂负载/化学计量比（TOC为39.1％和73.1％）获得NAP）。在10毫克的L二者操作^-1 NAP的，1.7毫升分钟^-1，50℃，pH值circumneutral。此外，它们的高消耗H ₂ O ₂效率（> 59.6％）和低浓度的溶出铁溶解（<0.28 mg L ^-1）在450分钟时发现的）表明催化剂具有很大的稳定性。此外，在不同的水基体上使用CWPO时，TOS 1260 min TOS中的NAP去除几乎完成（90.5％），而医院废水和废水处理厂废水样品中的NAP去除分别为64.9％和58.9％ 。我们的结果表明，采用易于制备的Fe ₃ O ₄ / MWCNTs进行连续CWPO具有潜力，可作为从不同水基质中快速去除NAP的有效方法。