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Synthesis and characterization of SrFeO 3-δ nanoparticles as antimicrobial agent
Journal of Sol-Gel Science and Technology ( IF 2.3 ) Pub Date : 2020-11-10 , DOI: 10.1007/s10971-020-05431-8
E. K. Abdel-Khalek , D. A. Rayan , Ahmed. A. Askar , M. I. A. Abdel Maksoud , H. H. El-Bahnasawy

In this work, synthesis and characterization of SrFeO3-δ nanoparticles as antimicrobial agent are presented. Structural characterization of SrFeO3-δ sample shows that it has a cubic (Pm3m) phase with minor tetragonal phase. The morphology of the SrFeO3-δ nanoparticles sample was characterized by a field emission scanning electron microscope (FE-SEM) and high resolution transmission electron microscopy (HRTEM). Mössbauer spectroscopy and X-ray photoelectron spectroscopy (XPS) results showed that the iron exists in oxidation states Fe3+, Fe3.5+, and Fe4+. The SrFeO3-δ nanoparticles sample exhibits energy band gap (Eg = 1.75 eV) which lies in the Visible region. Thermal and magnetic studies provide an evidence for ferroelectricity and antiferromagnetic with small amount of ferromagnetic in SrFeO3-δ nanoparticles sample, respectively. SrFeO3-δ nanoparticles sample showing powerful activity to fight both of tested Gram-positive, Gram-negative bacteria, and fungi strains. The antimicrobial activity as well as the minimal inhibitory concentration (MIC) and the minimum bactericidal concentration (MBC) of the SrFeO3-δ nanoparticles sample have been investigated.



中文翻译:

SrFeO3-δ纳米颗粒作为抗菌剂的合成与表征

在这项工作中,提出了作为抗菌剂的SrFeO3 纳米粒子的合成和表征。SrFeO3 样品的结构表征表明,它具有立方相(Pm3m)和次要四方相。通过场发射扫描电子显微镜(FE-SEM)和高分辨率透射电子显微镜(HRTEM)对SrFeO3 纳米粒子样品的形貌进行了表征。Mössbauer光谱和X射线光电子能谱(XPS)结果表明,铁以Fe 3+,Fe 3.5+和Fe 4+的氧化态存在。SrFeO3 纳米颗粒样品显示出能带隙(E g = 1.75 eV)位于可见区域。热学和磁学研究分别为SrFeO3 纳米颗粒样品中的少量铁磁提供了铁电和反铁磁的证据。SrFeO3 纳米颗粒样品显示出强大的活性,可与测试的革兰氏阳性菌,革兰氏阴性菌和真菌菌株对抗。研究了SrFeO3 纳米颗粒样品的抗菌活性以及最小抑菌浓度(MIC)和最小杀菌浓度(MBC)。

更新日期:2021-01-15
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