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Effect of annealing temperature on structure and high-temperature soft magnetic properties of (Fe0.9Co0.1)72.7Al0.8Si13.5Cu1Nb3B8V1 nanocrystalline alloy
Materials Research Bulletin ( IF 5.3 ) Pub Date : 2021-01-11 , DOI: 10.1016/j.materresbull.2021.111212
Yan Zhang , Zhi Wang , Xian-hua Li , Qian-qian Hao , Rui-min Shi

The structure and soft magnetic properties of nanocrystalline (Fe0.9Co0.1)72.7Al0.8Si13.5Cu1Nb3B8V1 alloy annealed at 510−690 °C were investigated by XRD patterns and initial permeability. It was observed that annealing within the ranges of 510−630 °C, only soft magnetic crystalline phase precipitated from the amorphous matrix. With the increase of annealing temperature, the grain size (D) and volume fraction of the crystalline phase (Vcry) both gradually increase from 11.9 nm to 13.7 nm and from 58 % to 89 % respectively. In the meanwhile, the thickness of the amorphous layer (Λ) gradually decreases from 2.37 nm to 0.54 nm. The change of initial permeability with temperature (μi -T curves) showed that the μi declines with increasing temperature. However, the rate of descent is different and the higher annealing temperature (Ta) corresponds to the slower attenuation of μi. The high-temperature μi gradually improves with annealing temperature (Ta) increasing up to 630 °C, and the higher μi of 1500 can be held up to 600 °C. However, the high-temperature μi dramatically deteriorates after annealing at 690 °C due to the precipitating hard magnetic phase from the residual amorphous matrix.



中文翻译:

退火温度对(Fe 0.9 Co 0.172.7 Al 0.8 Si 13.5 Cu 1 Nb 3 B 8 V 1纳米晶合金的结构和高温软磁性能的影响

通过X射线衍射图谱和初始磁导率研究了在510-690°C退火的纳米晶(Fe 0.9 Co 0.172.7 Al 0.8 Si 13.5 Cu 1 Nb 3 B 8 V 1合金的结构和软磁性能。观察到在510-630°C的范围内退火,只有软磁晶相从非晶态基质中析出。随着退火温度的升高,晶粒尺寸(D)和晶相的体积分数(V cry)分别从11.9 nm逐渐增加到13.7 nm和从58%逐渐增加到89%。同时,非晶层的厚度(Λ)从2.37nm逐渐减小至0.54nm。随温度的初始磁导率(变化μ-T曲线)表明,μ随着温度的增加而下降。然而,下降率是不同的,并且所述较高的退火温度(Ť一个)对应于较慢的衰减μ。高温μ随退火温度(逐渐提高Ť)提高到630℃,具有较高的μ1500的i可以保持在600°C。然而,高温μ在690℃下退火后的显着恶化,由于从剩余的无定形基质中的沉淀硬磁性相。

更新日期:2021-01-18
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