Effect of temperature and exfoliation time on the properties of chemically exfoliated MoS2 nanosheets,Chemical Communications

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Effect of temperature and exfoliation time on the properties of chemically exfoliated MoS2 nanosheets
Chemical Communications ( IF 4.3 ) Pub Date : 2020-11-20 , DOI: 10.1039/d0cc06792j
Iwona Janica _{1,

2,

3,

4,

5} , Daniel Iglesias _{6,

7,

8,

9,

10} , Stefano Ippolito _{6,

7,

8,

9,

10} , Artur Ciesielski _{3,

4,

5,

6,

11} , Paolo Samorì _{6,

7,

8,

9,

10}

Affiliation

A systematic investigation of the experimental conditions for the chemical exfoliation of MoS₂ using n-butyllithium as intercalating agent has been carried out to unravel the effect of reaction time and temperature for maximizing the percentage of monolayer thick-flakes and achieve a control over the content of metallic 1T vs. semiconductive 2H phases, thereby tuning the electrical properties of ultrathin MoS₂ few-layer thick films.

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