Recent progress in solid-state nuclear magnetic resonance of half-integer spin low-γ quadrupolar nuclei applied to inorganic materials,Magnetic Resonance in Chemistry

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Recent progress in solid-state nuclear magnetic resonance of half-integer spin low-γ quadrupolar nuclei applied to inorganic materials
Magnetic Resonance in Chemistry ( IF 1.9 ) Pub Date : 2020-11-18 , DOI: 10.1002/mrc.5116
Mark E Smith _{1,

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Affiliation

An overview is presented of recent progress in the solid-state nuclear magnetic resonance (NMR) observation of low-γ nuclei, with a focus on applications to inorganic materials. The technological and methodological advances in the last 20 years, which have underpinned the increased accessibility of low-γ nuclei for study by solid-state NMR techniques, are summarised, including improvements in hardware, pulse sequences and associated computational methods (e.g., first principles calculations and spectral simulation). Some of the key initial observations from inorganic materials of these nuclei are highlighted along with some recent (most within the last 10 years) illustrations of their application to such materials. A summary of other recent reviews of the study of low-γ nuclei by solid-state NMR is provided so that a comprehensive understanding of what has been achieved to date is available.

中文翻译：

半整数自旋低γ四极核固态核磁共振应用于无机材料的新进展

概述了低γ核的固态核磁共振 (NMR) 观察的最新进展，重点是无机材料的应用。总结了过去 20 年的技术和方法进步，这些进步支持了固态 NMR 技术研究中低γ核的可及性增加，包括硬件、脉冲序列和相关计算方法（例如，第一原理）的改进计算和光谱模拟）。这些核的无机材料的一些关键初步观察结果与一些最近（大多数在过去 10 年内）在这些材料上的应用的说明一起被突出显示。对低γ研究的其他近期评论的总结提供了通过固态 NMR 获得的原子核，以便全面了解迄今为止所取得的成就。

更新日期：2020-11-18

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